diethyl 4,4'-dithiobis

Base Information

Chemical Name:diethyl 4,4'-dithiobis
CAS No.:20057-83-4
Molecular Formula:C₁₈H₁₈O₄S₂
Molecular Weight:362.471
Hs Code.:

Synonyms:diethyl 4,4'-dithiobis

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Chemical Property of diethyl 4,4'-dithiobis

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Technology Process of diethyl 4,4'-dithiobis

There total 10 articles about diethyl 4,4'-dithiobis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 94-09-7
p-aminoethylbenzoate

: 20057-83-4
diethyl 4,4'-dithiobis

Guidance literature:: p-aminoethylbenzoate; With tetrafluoroboric acid; sodium nitrite; In water; acetone; at -20 - 0 ℃; for 0.333333h;

With carbon disulfide; tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate; In acetone; at 20 ℃; for 6h; Irradiation;
DOI:10.3762/bjoc.13.91

Reference yield: 89.0%

: 51934-41-9
4-iodobenzoic acid ethyl ester

: 20057-83-4
diethyl 4,4'-dithiobis

Guidance literature:: 4-iodobenzoic acid ethyl ester; With TurboGrignard; In tetrahydrofuran; at -20 ℃; for 0.5h; Schlenk technique;

With zinc dibromide; In tetrahydrofuran; at -40 ℃; for 0.5h; Schlenk technique;

With disulfur dichloride; In tetrahydrofuran; at -80 ℃; for 0.166667h; Schlenk technique;
DOI:10.1021/acs.orglett.8b03319