(1,2-bis(4-methoxyphenyl)-2-oxoethyl) 1-tert-butoxycarbonyl-4-allyl-4-piperidinecarboxylate

Base Information

Chemical Name:(1,2-bis(4-methoxyphenyl)-2-oxoethyl) 1-tert-butoxycarbonyl-4-allyl-4-piperidinecarboxylate
CAS No.:951745-39-4
Molecular Formula:C₃₀H₃₇NO₇
Molecular Weight:523.626
Hs Code.:

Synonyms:(1,2-bis(4-methoxyphenyl)-2-oxoethyl) 1-tert-butoxycarbonyl-4-allyl-4-piperidinecarboxylate

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Chemical Property of (1,2-bis(4-methoxyphenyl)-2-oxoethyl) 1-tert-butoxycarbonyl-4-allyl-4-piperidinecarboxylate

Chemical Property:

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Technology Process of (1,2-bis(4-methoxyphenyl)-2-oxoethyl) 1-tert-butoxycarbonyl-4-allyl-4-piperidinecarboxylate

There total 3 articles about (1,2-bis(4-methoxyphenyl)-2-oxoethyl) 1-tert-butoxycarbonyl-4-allyl-4-piperidinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 119-52-8
4,4'-dimethoxybenzoin

: 426842-70-8
4-allyl-1-(tert-butoxycarbonyl)piperidine-4-carboxylic acid

: 951745-39-4
(1,2-bis(4-methoxyphenyl)-2-oxoethyl) 1-tert-butoxycarbonyl-4-allyl-4-piperidinecarboxylate

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; toluene; at 20 ℃; for 3h;

Reference yield:

: 676341-47-2
allyl 1-tert-butoxycarbonyl-4-piperidinecarboxylate

: 951745-39-4
(1,2-bis(4-methoxyphenyl)-2-oxoethyl) 1-tert-butoxycarbonyl-4-allyl-4-piperidinecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C

1.2: 1 h / -78 - 20 °C

2.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran; toluene / 3 h / 20 °C

With di-isopropyl azodicarboxylate; triphenylphosphine; lithium hexamethyldisilazane; In tetrahydrofuran; toluene;

Reference yield:

: 84358-13-4,174286-31-8
N-[(tert-butoxy)carbonyl]piperidine-4-carboxylic acid

: 951745-39-4
(1,2-bis(4-methoxyphenyl)-2-oxoethyl) 1-tert-butoxycarbonyl-4-allyl-4-piperidinecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 20 °C

2.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C

2.2: 1 h / -78 - 20 °C

3.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran; toluene / 3 h / 20 °C

With di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; lithium hexamethyldisilazane; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;