C₂₂H₃₉⁽²⁾HOSi₂

Base Information

• Chemical Name: C₂₂H₃₉⁽²⁾HOSi₂
• CAS No.: 1555710-31-0
• Molecular Formula: C₂₂H₄₀OSi₂
• Molecular Weight: 377.722

Synonyms:C₂₂H₃₉⁽²⁾HOSi₂

Chemical Property of C₂₂H₃₉⁽²⁾HOSi₂

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Technology Process of C₂₂H₃₉⁽²⁾HOSi₂

There total 1 articles about C₂₂H₃₉⁽²⁾HOSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

3,3-bis(triethylsilyl) benzyl enol ether → C22H39(2)HOSi2 (1555710-31-0)

Guidance literature:

3,3-bis(triethylsilyl) benzyl enol ether; With N,N,N,N,N,N-hexamethylphosphoric triamide; tert.-butyl lithium; In tetrahydrofuran; pentane; at -78 ℃; for 1.5h; Inert atmosphere;

With water-d2; In tetrahydrofuran; pentane; at -78 ℃; for 0.166667h; Inert atmosphere;

DOI:10.1021/ol4036402

Reference yield: 99.0%

C22H39(2)HOSi2 (1555710-31-0) + 3-chloroprop-1-ene (107-05-1) → C25H43(2)HOSi2 (1606174-97-3)

Guidance literature:

C₂₂H₃₉⁽²⁾HOSi₂; With N,N,N,N,N,N-hexamethylphosphoric triamide; tert.-butyl lithium; In tetrahydrofuran; pentane; at -78 ℃; for 1.5h; Inert atmosphere;

3-chloroprop-1-ene; In tetrahydrofuran; pentane; at -78 ℃; for 0.166667h; Inert atmosphere;

DOI:10.1039/c4ob00139g

Reference yield: 85.0%

C22H39(2)HOSi2 (1555710-31-0) + 4-methoxy-benzaldehyde (123-11-5) → C30H47(2)HO3Si2

Guidance literature:

C₂₂H₃₉⁽²⁾HOSi₂; With N,N,N,N,N,N-hexamethylphosphoric triamide; tert.-butyl lithium; In tetrahydrofuran; pentane; at -78 ℃; for 1.5h; Inert atmosphere;

4-methoxy-benzaldehyde; In tetrahydrofuran; pentane; at -78 ℃; for 0.166667h; diastereoselective reaction; Inert atmosphere;

DOI:10.1021/ol4036402

Downstream raw materials:

C₂₅H₄₃⁽²⁾HOSi₂

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