4-nitrophenyl pent-4-enoate

Base Information

• Chemical Name: 4-nitrophenyl pent-4-enoate
• CAS No.: 51231-11-9
• Molecular Formula: C₁₁H₁₁NO₄
• Molecular Weight: 221.213
• Mol file: 51231-11-9.mol

Synonyms:4-nitrophenyl pent-4-enoate

Chemical Property of 4-nitrophenyl pent-4-enoate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 4-nitrophenyl pent-4-enoate

There total 4 articles about 4-nitrophenyl pent-4-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + pent-4-enoic acid (591-80-0) → 4-nitrophenyl pent-4-enoate (51231-11-9)

Guidance literature:

With dmap; diisopropyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; for 1.16667h;

DOI:10.1021/acsmedchemlett.9b00643

Reference yield: 89.0%

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + pent-4-enoyl chloride (39716-58-0) → 4-nitrophenyl pent-4-enoate (51231-11-9)

Guidance literature:

With potassium hydroxide; In water; at 5 ℃;

DOI:10.1007/s10847-009-9711-x

Reference yield: 87.0%

pent-4-enoic acid (591-80-0) + 4-Nitrophenyl chloroformate (7693-46-1) → 4-nitrophenyl pent-4-enoate (51231-11-9)

Guidance literature:

pent-4-enoic acid; With triethylamine; In dichloromethane; for 0.166667h; Inert atmosphere;

4-Nitrophenyl chloroformate; In dichloromethane; at 20 ℃; Inert atmosphere;

DOI:10.1039/c4cc09003a

upstream raw materials:

4-nitro-phenol

pent-4-enoyl chloride

pent-4-enoic acid

4-Nitrophenyl chloroformate

Downstream raw materials:

buta-1,3-diene