2-((6-((2,6-diisopropylphenyl)amino)-6-oxohexyl)thio)benzo[d]oxazole-5-carboxylic acid

Base Information

Chemical Name:2-((6-((2,6-diisopropylphenyl)amino)-6-oxohexyl)thio)benzo[d]oxazole-5-carboxylic acid
CAS No.:213684-91-4
Molecular Formula:C₂₆H₃₂N₂O₄S
Molecular Weight:468.617
Hs Code.:

Synonyms:2-((6-((2,6-diisopropylphenyl)amino)-6-oxohexyl)thio)benzo[d]oxazole-5-carboxylic acid

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Chemical Property of 2-((6-((2,6-diisopropylphenyl)amino)-6-oxohexyl)thio)benzo[d]oxazole-5-carboxylic acid

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Technology Process of 2-((6-((2,6-diisopropylphenyl)amino)-6-oxohexyl)thio)benzo[d]oxazole-5-carboxylic acid

There total 8 articles about 2-((6-((2,6-diisopropylphenyl)amino)-6-oxohexyl)thio)benzo[d]oxazole-5-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 213684-90-3
methyl 2-((6-((2,6-diisopropylphenyl)amino)-6-oxohexyl)thio)benzo[d]oxazole-5-carboxylate

: 213684-91-4
2-((6-((2,6-diisopropylphenyl)amino)-6-oxohexyl)thio)benzo[d]oxazole-5-carboxylic acid

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; water; tert-butyl alcohol; at 20 ℃; for 12h;
DOI:10.1016/j.bmc.2018.06.024

Reference yield:

: 199592-72-8
6-bromo-N-(2,6-diisopropylphenyl)hexanamide

: 213684-91-4
2-((6-((2,6-diisopropylphenyl)amino)-6-oxohexyl)thio)benzo[d]oxazole-5-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; 18-crown-6 ether / N,N-dimethyl-formamide / 2 h / 80 °C

2: lithium hydroxide / tetrahydrofuran; water; tert-butyl alcohol / 12 h / 20 °C

With 18-crown-6 ether; potassium carbonate; lithium hydroxide; In tetrahydrofuran; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/j.bmc.2018.06.024

Reference yield:

: 4224-70-8
6-bromohexanoic acid

: 213684-91-4
2-((6-((2,6-diisopropylphenyl)amino)-6-oxohexyl)thio)benzo[d]oxazole-5-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 12 h / 0 - 20 °C

2: potassium carbonate; 18-crown-6 ether / N,N-dimethyl-formamide / 2 h / 80 °C

3: lithium hydroxide / tetrahydrofuran; water; tert-butyl alcohol / 12 h / 20 °C

With 18-crown-6 ether; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide; In tetrahydrofuran; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/j.bmc.2018.06.024