methyl 2-((6-((2,6-diisopropylphenyl)amino)-6-oxohexyl)thio)benzo[d]oxazole-5-carboxylate

Base Information

Chemical Name:methyl 2-((6-((2,6-diisopropylphenyl)amino)-6-oxohexyl)thio)benzo[d]oxazole-5-carboxylate
CAS No.:213684-90-3
Molecular Formula:C₂₇H₃₄N₂O₄S
Molecular Weight:482.644
Hs Code.:

Synonyms:methyl 2-((6-((2,6-diisopropylphenyl)amino)-6-oxohexyl)thio)benzo[d]oxazole-5-carboxylate

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Chemical Property of methyl 2-((6-((2,6-diisopropylphenyl)amino)-6-oxohexyl)thio)benzo[d]oxazole-5-carboxylate

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Technology Process of methyl 2-((6-((2,6-diisopropylphenyl)amino)-6-oxohexyl)thio)benzo[d]oxazole-5-carboxylate

There total 5 articles about methyl 2-((6-((2,6-diisopropylphenyl)amino)-6-oxohexyl)thio)benzo[d]oxazole-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 199592-72-8
6-bromo-N-(2,6-diisopropylphenyl)hexanamide

: 72730-39-3
methyl 2-sulfanyl-1,3-benzoxazole-5-carboxylate

: 213684-90-3
methyl 2-((6-((2,6-diisopropylphenyl)amino)-6-oxohexyl)thio)benzo[d]oxazole-5-carboxylate

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 2h;
DOI:10.1016/j.bmc.2018.06.024

Reference yield:

: 4224-70-8
6-bromohexanoic acid

: 213684-90-3
methyl 2-((6-((2,6-diisopropylphenyl)amino)-6-oxohexyl)thio)benzo[d]oxazole-5-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 12 h / 0 - 20 °C

2: potassium carbonate; 18-crown-6 ether / N,N-dimethyl-formamide / 2 h / 80 °C

With 18-crown-6 ether; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2018.06.024

Reference yield:

: 536-25-4
methyl 3-amino-4-hydroxybenzoate

: 213684-90-3
methyl 2-((6-((2,6-diisopropylphenyl)amino)-6-oxohexyl)thio)benzo[d]oxazole-5-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 0.08 h / 20 °C

2: potassium carbonate; 18-crown-6 ether / N,N-dimethyl-formamide / 2 h / 80 °C

With 18-crown-6 ether; potassium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2018.06.024