2,2-difluoro-6-(furan-2-yl)-4-phenyl-2H-1,3,2-dioxaborinin-1-ium-2-uide

Base Information

Chemical Name:2,2-difluoro-6-(furan-2-yl)-4-phenyl-2H-1,3,2-dioxaborinin-1-ium-2-uide
CAS No.:1233878-88-0
Molecular Formula:C₁₃H₉BF₂O₃
Molecular Weight:262.02
Hs Code.:

Synonyms:2,2-difluoro-6-(furan-2-yl)-4-phenyl-2H-1,3,2-dioxaborinin-1-ium-2-uide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2-difluoro-6-(furan-2-yl)-4-phenyl-2H-1,3,2-dioxaborinin-1-ium-2-uide

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Technology Process of 2,2-difluoro-6-(furan-2-yl)-4-phenyl-2H-1,3,2-dioxaborinin-1-ium-2-uide

There total 2 articles about 2,2-difluoro-6-(furan-2-yl)-4-phenyl-2H-1,3,2-dioxaborinin-1-ium-2-uide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 5910-23-6
1-furan-2-yl-3-phenyl-propane-1,3-dione

: 109-63-7
boron trifluoride diethyl etherate

: 1233878-88-0
2,2-difluoro-6-(furan-2-yl)-4-phenyl-2H-1,3,2-dioxaborinin-1-ium-2-uide

Guidance literature:: In dichloromethane; at 60 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c6ra20489a

Reference yield:

: 611-13-2
2-furoic acid methyl ester

: 98-86-2
acetophenone

: 1233878-88-0
2,2-difluoro-6-(furan-2-yl)-4-phenyl-2H-1,3,2-dioxaborinin-1-ium-2-uide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / tetrahydrofuran / 24 h / 66 °C / Inert atmosphere

2: dichloromethane / 2 h / 60 °C / Inert atmosphere

With sodium hydride; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c6ra20489a