N-Formyl-N-(2,3,4-tri-O-pivaloyl-β-L-fucopyranosyl)-L-(4-chlorophenyl)glycine N'-tert-butylamide

Base Information

Chemical Name:N-Formyl-N-(2,3,4-tri-O-pivaloyl-β-L-fucopyranosyl)-L-(4-chlorophenyl)glycine N'-tert-butylamide
CAS No.:138892-02-1
Molecular Formula:C₃₄H₅₁ClN₂O₉
Molecular Weight:667.24
Hs Code.:

Synonyms:N-Formyl-N-(2,3,4-tri-O-pivaloyl-β-L-fucopyranosyl)-L-(4-chlorophenyl)glycine N'-tert-butylamide

Suppliers and Price of N-Formyl-N-(2,3,4-tri-O-pivaloyl-β-L-fucopyranosyl)-L-(4-chlorophenyl)glycine N'-tert-butylamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-Formyl-N-(2,3,4-tri-O-pivaloyl-β-L-fucopyranosyl)-L-(4-chlorophenyl)glycine N'-tert-butylamide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of N-Formyl-N-(2,3,4-tri-O-pivaloyl-β-L-fucopyranosyl)-L-(4-chlorophenyl)glycine N'-tert-butylamide

There total 7 articles about N-Formyl-N-(2,3,4-tri-O-pivaloyl-β-L-fucopyranosyl)-L-(4-chlorophenyl)glycine N'-tert-butylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 64-18-6
formic acid

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 104-88-1
4-chlorobenzaldehyde

: 138891-95-9
2,3,4-Tri-O-pivaloyl-β-L-fucopyranosylamine

: 138892-02-1
N-Formyl-N-(2,3,4-tri-O-pivaloyl-β-L-fucopyranosyl)-L-(4-chlorophenyl)glycine N'-tert-butylamide

: 138892-02-1
N-Formyl-N-(2,3,4-tri-O-pivaloyl-β-L-fucopyranosyl)-D-(4-chlorophenyl)glycine N'-tert-butylamide

Guidance literature:: With zinc(II) chloride; In tetrahydrofuran; at -24 ℃; for 24h; Yields of byproduct given;
DOI:10.1055/s-1991-26641

Reference yield: 86.0%

: 64-18-6
formic acid

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 104-88-1
4-chlorobenzaldehyde

: 138891-95-9
2,3,4-Tri-O-pivaloyl-β-L-fucopyranosylamine

: 138892-02-1
N-Formyl-N-(2,3,4-tri-O-pivaloyl-β-L-fucopyranosyl)-L-(4-chlorophenyl)glycine N'-tert-butylamide

: 138892-02-1
N-Formyl-N-(2,3,4-tri-O-pivaloyl-β-L-fucopyranosyl)-D-(4-chlorophenyl)glycine N'-tert-butylamide

Guidance literature:: With zinc(II) chloride; In tetrahydrofuran; at -24 ℃; for 24h; Yields of byproduct given;
DOI:10.1055/s-1991-26641

Reference yield:

: 3282-30-2
pivaloyl chloride

: 138892-02-1
N-Formyl-N-(2,3,4-tri-O-pivaloyl-β-L-fucopyranosyl)-L-(4-chlorophenyl)glycine N'-tert-butylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / pyridine / 24 h / Ambient temperature

2: 91 percent / H₂ / Raney Ni / methanol; CH₂Cl₂ / 3 h / 760 Torr / Ambient temperature

3: 86 percent / ZnCl₂ / tetrahydrofuran / 24 h / -24 °C

With pyridine; hydrogen; zinc(II) chloride; nickel; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1055/s-1991-26641