(Z)-1,2-Bis(methylthio)-1,2-diphenylethen

Base Information

Chemical Name:(Z)-1,2-Bis(methylthio)-1,2-diphenylethen
CAS No.:57094-00-5
Molecular Formula:C₁₆H₁₆S₂
Molecular Weight:272.435
Hs Code.:

Synonyms:(Z)-1,2-Bis(methylthio)-1,2-diphenylethen

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-1,2-Bis(methylthio)-1,2-diphenylethen

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Technology Process of (Z)-1,2-Bis(methylthio)-1,2-diphenylethen

There total 10 articles about (Z)-1,2-Bis(methylthio)-1,2-diphenylethen which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.5%

: 75-16-1
methylmagnesium bromide

: 28984-20-5
bis(1,2-diphenylethylene-1,2-ditholate) nickel(IV)

: 129261-17-2,129261-18-3,129261-16-1,67430-35-7
C₃₀H₂₆NiS₄

: {Ni(S₂C₂Ph₂)}(x)

: 57094-00-5
(Z)-1,2-Bis(methylthio)-1,2-diphenylethen

Guidance literature:: With CH₃I; In tetrahydrofuran; byproducts: C2H6, CH4; suspension of Ni-compound flushed with dry argon, CH3MgBr added dropwise, after the reaction was complete (about 30 min) CH3I added dropwise; evaporated to dryness after 12 h, extracted (n-hexane), treated (CH2Cl2), recrystd. (toluene/hexane), n-hexane added to the filtrate; elem. anal., NMR, GLPC;

Reference yield: 56.0%

: 2168-78-7
methyl dithiobenzoate

: 74-88-4
methyl iodide

: 14252-44-9
bis(methylthio)phenylmethane

: 57094-00-5
(Z)-1,2-Bis(methylthio)-1,2-diphenylethen

: 57093-97-7
(E)-1,2-Bis(methylthio)-1,2-diphenylethen

Guidance literature:: With tetrapropylammonium perruthennate; Product distribution; 1) electroreduction, Hg-cathode, acetonitrile, 20 deg C, 5 min, 2) 50 deg C; further reagents, further educts, further solvents, further products;

Reference yield: 19.9%

: 75-16-1
methylmagnesium bromide

: 28984-20-5
bis(1,2-diphenylethylene-1,2-ditholate) nickel(IV)

: 129261-81-0
bis(trans-(methylthio)stilbenethiolato)nickel(II)*CH₂Cl₂

: {Ni(S₂C₂Ph₂)}(x)

: 57094-00-5
(Z)-1,2-Bis(methylthio)-1,2-diphenylethen

Guidance literature:: With CH₃I; In tetrahydrofuran; byproducts: C2H6, CH4; suspension of Ni-compound flushed with dry argon, CH3MgBr added dropwise, after the reaction was complete (about 30 min) CH3I added dropwise; evaporated to dryness after 12 h, extracted (n-hexane), treated (CH2Cl2), n-hexane added to the filtrate; elem. anal., NMR, GLPC;