12-cyclohexyl-2-(dimethylcarbamoyl)-1-{[ethyl(methyl)amino]methyl}-5,6-dihydro-4H-[1,5]diazocino[1,2-a:5,4,3-h'i']diindole-9-carboxylic acid

Base Information

Chemical Name:12-cyclohexyl-2-(dimethylcarbamoyl)-1-{[ethyl(methyl)amino]methyl}-5,6-dihydro-4H-[1,5]diazocino[1,2-a:5,4,3-h'i']diindole-9-carboxylic acid
CAS No.:1169854-71-0
Molecular Formula:C₃₃H₄₀N₄O₃
Molecular Weight:540.706
Hs Code.:

Synonyms:12-cyclohexyl-2-(dimethylcarbamoyl)-1-{[ethyl(methyl)amino]methyl}-5,6-dihydro-4H-[1,5]diazocino[1,2-a:5,4,3-h'i']diindole-9-carboxylic acid

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Chemical Property of 12-cyclohexyl-2-(dimethylcarbamoyl)-1-{[ethyl(methyl)amino]methyl}-5,6-dihydro-4H-[1,5]diazocino[1,2-a:5,4,3-h'i']diindole-9-carboxylic acid

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Technology Process of 12-cyclohexyl-2-(dimethylcarbamoyl)-1-{[ethyl(methyl)amino]methyl}-5,6-dihydro-4H-[1,5]diazocino[1,2-a:5,4,3-h'i']diindole-9-carboxylic acid

There total 2 articles about 12-cyclohexyl-2-(dimethylcarbamoyl)-1-{[ethyl(methyl)amino]methyl}-5,6-dihydro-4H-[1,5]diazocino[1,2-a:5,4,3-h'i']diindole-9-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1169857-21-9
methyl 12-cyclohexyl-2-(dimethylcarbamoyl)-1-{[ethyl(methyl)amino]methyl}-5,6-dihydro-4H-[1,5]diazocino[1,2-a:5,4,3-h'i']diindole-9-carboxylate

: 1169854-71-0
12-cyclohexyl-2-(dimethylcarbamoyl)-1-{[ethyl(methyl)amino]methyl}-5,6-dihydro-4H-[1,5]diazocino[1,2-a:5,4,3-h'i']diindole-9-carboxylic acid

Guidance literature:: methyl 12-cyclohexyl-2-(dimethylcarbamoyl)-1-{[ethyl(methyl)amino]methyl}-5,6-dihydro-4H-[1,5]diazocino[1,2-a:5,4,3-h'i']diindole-9-carboxylate; With water; lithium hydroxide; In tetrahydrofuran; methanol; at 58 ℃; for 3h;

With trifluoroacetic acid;

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 624-78-2
N-Ethylmethylamine

: 1169854-97-0
C₂₉H₃₁N₃O₃

: 1169854-71-0
12-cyclohexyl-2-(dimethylcarbamoyl)-1-{[ethyl(methyl)amino]methyl}-5,6-dihydro-4H-[1,5]diazocino[1,2-a:5,4,3-h'i']diindole-9-carboxylic acid

Guidance literature:: formaldehyd; N-Ethylmethylamine; With acetic acid; at 20 ℃; for 0.166667h;

C₂₉H₃₁N₃O₃; at 60 ℃; for 2h;

Reference yield:

: 3984-14-3
N,N-dimethylsulfamide

: 1169854-71-0
12-cyclohexyl-2-(dimethylcarbamoyl)-1-{[ethyl(methyl)amino]methyl}-5,6-dihydro-4H-[1,5]diazocino[1,2-a:5,4,3-h'i']diindole-9-carboxylic acid

: 1169854-82-3
C₃₅H₄₆N₆O₄S

Guidance literature:: 12-cyclohexyl-2-(dimethylcarbamoyl)-1-{[ethyl(methyl)amino]methyl}-5,6-dihydro-4H-[1,5]diazocino[1,2-a:5,4,3-h'i']diindole-9-carboxylic acid; With dmap; HATU; In tetrahydrofuran;

N,N-dimethylsulfamide; In tetrahydrofuran; at 70 ℃;