2,2-dimethylpropanoic acid 1-[bis(methylsulfanyl)methyl]-3-{(but-3-enoyl)[2-(3,4-dimethoxyphenyl)ethyl]amino}-3-oxopropyl ester

Base Information

Chemical Name:2,2-dimethylpropanoic acid 1-[bis(methylsulfanyl)methyl]-3-{(but-3-enoyl)[2-(3,4-dimethoxyphenyl)ethyl]amino}-3-oxopropyl ester
CAS No.:496863-42-4
Molecular Formula:C₂₅H₃₇NO₆S₂
Molecular Weight:511.704
Hs Code.:

Synonyms:2,2-dimethylpropanoic acid 1-[bis(methylsulfanyl)methyl]-3-{(but-3-enoyl)[2-(3,4-dimethoxyphenyl)ethyl]amino}-3-oxopropyl ester

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Chemical Property of 2,2-dimethylpropanoic acid 1-[bis(methylsulfanyl)methyl]-3-{(but-3-enoyl)[2-(3,4-dimethoxyphenyl)ethyl]amino}-3-oxopropyl ester

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Technology Process of 2,2-dimethylpropanoic acid 1-[bis(methylsulfanyl)methyl]-3-{(but-3-enoyl)[2-(3,4-dimethoxyphenyl)ethyl]amino}-3-oxopropyl ester

There total 4 articles about 2,2-dimethylpropanoic acid 1-[bis(methylsulfanyl)methyl]-3-{(but-3-enoyl)[2-(3,4-dimethoxyphenyl)ethyl]amino}-3-oxopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1470-91-3
but-3-enoyl chloride

: 496863-41-3
2,2-dimethylpropanoic acid 1-({[2-(3,4-dimethoxyphenyl)ethyl]carbamoyl}methyl)-2,2-bis(methylsulfanyl)ethyl ester

: 496863-42-4
2,2-dimethylpropanoic acid 1-[bis(methylsulfanyl)methyl]-3-{(but-3-enoyl)[2-(3,4-dimethoxyphenyl)ethyl]amino}-3-oxopropyl ester

Guidance literature:: With molecular sieve; In dichloromethane; at 20 ℃;
DOI:10.3987/COM-02-S(M)12

Reference yield:

: 6275-29-2
N-[2-(3,4-dimethoxyphenyl)ethyl]acetamide

: 496863-42-4
2,2-dimethylpropanoic acid 1-[bis(methylsulfanyl)methyl]-3-{(but-3-enoyl)[2-(3,4-dimethoxyphenyl)ethyl]amino}-3-oxopropyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 93 percent / powdered molecular sieves / CH₂Cl₂ / 20 °C

2.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 1 h / -40 °C

2.2: 57 percent / tetrahydrofuran / 3.5 h / -75 °C

3.1: 81 percent / powdered molecular sieves / CH₂Cl₂ / 20 °C

With n-butyllithium; molecular sieve; diisopropylamine; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.3987/COM-02-S(M)12

Reference yield:

: 3282-30-2
pivaloyl chloride

: 496863-42-4
2,2-dimethylpropanoic acid 1-[bis(methylsulfanyl)methyl]-3-{(but-3-enoyl)[2-(3,4-dimethoxyphenyl)ethyl]amino}-3-oxopropyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 93 percent / powdered molecular sieves / CH₂Cl₂ / 20 °C

2.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 1 h / -40 °C

2.2: 57 percent / tetrahydrofuran / 3.5 h / -75 °C

3.1: 81 percent / powdered molecular sieves / CH₂Cl₂ / 20 °C

With n-butyllithium; molecular sieve; diisopropylamine; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.3987/COM-02-S(M)12