(2Z)-{[(2-amino-1,3-thiazol-4-yl)methoxy]imino}(3-methoxyphenyl)acetonitrile

Base Information

Chemical Name:(2Z)-{[(2-amino-1,3-thiazol-4-yl)methoxy]imino}(3-methoxyphenyl)acetonitrile
CAS No.:1446194-09-7
Molecular Formula:C₁₃H₁₂N₄O₂S
Molecular Weight:288.33
Hs Code.:

Synonyms:(2Z)-{[(2-amino-1,3-thiazol-4-yl)methoxy]imino}(3-methoxyphenyl)acetonitrile

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Chemical Property of (2Z)-{[(2-amino-1,3-thiazol-4-yl)methoxy]imino}(3-methoxyphenyl)acetonitrile

Chemical Property:

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Technology Process of (2Z)-{[(2-amino-1,3-thiazol-4-yl)methoxy]imino}(3-methoxyphenyl)acetonitrile

There total 1 articles about (2Z)-{[(2-amino-1,3-thiazol-4-yl)methoxy]imino}(3-methoxyphenyl)acetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1446194-13-3
(2Z)-(hydroxyimino)(3-methoxyphenyl)acetonitrile

: 59608-97-8
4-(chloromethyl)thiazol-2-amine hydrochloride

: 1446194-09-7
(2Z)-{[(2-amino-1,3-thiazol-4-yl)methoxy]imino}(3-methoxyphenyl)acetonitrile

Guidance literature:: With caesium carbonate; potassium iodide; In N,N-dimethyl-formamide; acetonitrile; at 20 ℃; for 8h;

Reference yield: 69.0%

: 1446194-09-7
(2Z)-{[(2-amino-1,3-thiazol-4-yl)methoxy]imino}(3-methoxyphenyl)acetonitrile

: 4229-44-1
N-methylhydroxyamine hydrochloride

: 1446194-10-0
(2Z)-2-{[(2-amino-1,3-thiazol-4-yl)methoxy]imino}-N-hydroxy-N-methyl-2-(3-methoxyphenyl)ethanimidamide

Guidance literature:: With potassium carbonate; In water; isopropyl alcohol; at 80 ℃; for 2h;

Reference yield:

: 1446194-09-7
(2Z)-{[(2-amino-1,3-thiazol-4-yl)methoxy]imino}(3-methoxyphenyl)acetonitrile

: 1446193-36-7
cyclohexyl {4-[({[(Z)-(3-methoxyphenyl)(2-methyl-5-oxo-2,5-dihydro-1,2,4-oxadiazol-3-yl)methylene]amino}oxy)methyl]-1,3-thiazol-2-yl}carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / isopropyl alcohol; water / 2 h / 80 °C

2.1: triethylamine / N,N-dimethyl-formamide / 0 °C

3.1: pyridine / acetonitrile / 2 h / 20 °C

3.2: 15 h / Reflux

With pyridine; potassium carbonate; triethylamine; In water; N,N-dimethyl-formamide; isopropyl alcohol; acetonitrile;