(2Z)-2-{[(2-amino-1,3-thiazol-4-yl)methoxy]imino}-N-hydroxy-N-methyl-2-(3-methoxyphenyl)ethanimidamide

Base Information

Chemical Name:(2Z)-2-{[(2-amino-1,3-thiazol-4-yl)methoxy]imino}-N-hydroxy-N-methyl-2-(3-methoxyphenyl)ethanimidamide
CAS No.:1446194-10-0
Molecular Formula:C₁₄H₁₇N₅O₃S
Molecular Weight:335.387
Hs Code.:

Synonyms:(2Z)-2-{[(2-amino-1,3-thiazol-4-yl)methoxy]imino}-N-hydroxy-N-methyl-2-(3-methoxyphenyl)ethanimidamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2Z)-2-{[(2-amino-1,3-thiazol-4-yl)methoxy]imino}-N-hydroxy-N-methyl-2-(3-methoxyphenyl)ethanimidamide

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Technology Process of (2Z)-2-{[(2-amino-1,3-thiazol-4-yl)methoxy]imino}-N-hydroxy-N-methyl-2-(3-methoxyphenyl)ethanimidamide

There total 2 articles about (2Z)-2-{[(2-amino-1,3-thiazol-4-yl)methoxy]imino}-N-hydroxy-N-methyl-2-(3-methoxyphenyl)ethanimidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1446194-09-7
(2Z)-{[(2-amino-1,3-thiazol-4-yl)methoxy]imino}(3-methoxyphenyl)acetonitrile

: 4229-44-1
N-methylhydroxyamine hydrochloride

: 1446194-10-0
(2Z)-2-{[(2-amino-1,3-thiazol-4-yl)methoxy]imino}-N-hydroxy-N-methyl-2-(3-methoxyphenyl)ethanimidamide

Guidance literature:: With potassium carbonate; In water; isopropyl alcohol; at 80 ℃; for 2h;

Reference yield:

: 1446194-13-3
(2Z)-(hydroxyimino)(3-methoxyphenyl)acetonitrile

: 1446194-10-0
(2Z)-2-{[(2-amino-1,3-thiazol-4-yl)methoxy]imino}-N-hydroxy-N-methyl-2-(3-methoxyphenyl)ethanimidamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium iodide; caesium carbonate / acetonitrile; N,N-dimethyl-formamide / 8 h / 20 °C

2: potassium carbonate / isopropyl alcohol; water / 2 h / 80 °C

With potassium carbonate; caesium carbonate; potassium iodide; In water; N,N-dimethyl-formamide; isopropyl alcohol; acetonitrile;