[1-({2-[1-(tert-butyl-dimethyl-silanyloxy)-2,2,2-trifluoro-1-trifluoromethyl-ethyl]-phenylselanyl}-phenyl-methyl)-2,2,2-trifluoro-1-trifluoromethyl-ethyl]-phenyl-amine

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Chemical Name:[1-({2-[1-(tert-butyl-dimethyl-silanyloxy)-2,2,2-trifluoro-1-trifluoromethyl-ethyl]-phenylselanyl}-phenyl-methyl)-2,2,2-trifluoro-1-trifluoromethyl-ethyl]-phenyl-amine
CAS No.:334866-55-6
Molecular Formula:C₃₁H₃₁F₁₂NOSeSi
Molecular Weight:768.62
Hs Code.:

[1-({2-[1-(<i>tert</i>-butyl-dimethyl-silanyloxy)-2,2,2-trifluoro-1-trifluoromethyl-ethyl]-phenylselanyl}-phenyl-methyl)-2,2,2-trifluoro-1-trifluoromethyl-ethyl]-phenyl-amine

Synonyms:[1-({2-[1-(tert-butyl-dimethyl-silanyloxy)-2,2,2-trifluoro-1-trifluoromethyl-ethyl]-phenylselanyl}-phenyl-methyl)-2,2,2-trifluoro-1-trifluoromethyl-ethyl]-phenyl-amine

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Chemical Property of [1-({2-[1-(tert-butyl-dimethyl-silanyloxy)-2,2,2-trifluoro-1-trifluoromethyl-ethyl]-phenylselanyl}-phenyl-methyl)-2,2,2-trifluoro-1-trifluoromethyl-ethyl]-phenyl-amine

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Technology Process of [1-({2-[1-(tert-butyl-dimethyl-silanyloxy)-2,2,2-trifluoro-1-trifluoromethyl-ethyl]-phenylselanyl}-phenyl-methyl)-2,2,2-trifluoro-1-trifluoromethyl-ethyl]-phenyl-amine

There total 1 articles about [1-({2-[1-(tert-butyl-dimethyl-silanyloxy)-2,2,2-trifluoro-1-trifluoromethyl-ethyl]-phenylselanyl}-phenyl-methyl)-2,2,2-trifluoro-1-trifluoromethyl-ethyl]-phenyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 2002-95-1
N-(hexafluoroisopropylidene)aniline

: 195516-38-2
benzyl 2-[1-(tert-butyldimethylsiloxy)-2,2,2-trifluoro-1-(trifluoromethyl)-ethyl]phenyl selenide

: 334866-55-6
[1-({2-[1-(tert-butyl-dimethyl-silanyloxy)-2,2,2-trifluoro-1-trifluoromethyl-ethyl]-phenylselanyl}-phenyl-methyl)-2,2,2-trifluoro-1-trifluoromethyl-ethyl]-phenyl-amine

Guidance literature:: benzyl 2-[1-(tert-butyldimethylsiloxy)-2,2,2-trifluoro-1-(trifluoromethyl)-ethyl]phenyl selenide; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 2h;

N-(hexafluoroisopropylidene)aniline; In tetrahydrofuran; at -78 ℃; for 10h; Further stages.;
DOI:10.1021/ol007015m

Reference yield:

: 334866-55-6
[1-({2-[1-(tert-butyl-dimethyl-silanyloxy)-2,2,2-trifluoro-1-trifluoromethyl-ethyl]-phenylselanyl}-phenyl-methyl)-2,2,2-trifluoro-1-trifluoromethyl-ethyl]-phenyl-amine

: 100-52-7
benzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: n-Bu₄NF / tetrahydrofuran / 0.5 h / 0 °C

2: 40 percent / mCPBA; CHCl₃ / 0.5 h / 0 °C

3: 16 percent Spectr_. / various solvent(s) / 210 °C

With chloroform; tetrabutyl ammonium fluoride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran;
DOI:10.1021/ol007015m