1-Tert-butyl-2-(diphenylmethylidene)hydrazine

Base Information

Chemical Name:1-Tert-butyl-2-(diphenylmethylidene)hydrazine
CAS No.:24398-53-6
Molecular Formula:C17H20 N2
Molecular Weight:252.359
Hs Code.:
NSC Number:94926
DSSTox Substance ID:DTXSID20294166
Mol file:24398-53-6.mol

Synonyms:24398-53-6;1-tert-butyl-2-(diphenylmethylidene)hydrazine;N-(benzhydrylideneamino)-2-methylpropan-2-amine;Methanone, diphenyl-,(1,1-dimethylethyl)hydrazone (9CI);NSC94926;NCIOpen2_006092;DTXSID20294166;NSC-94926

Suppliers and Price of 1-Tert-butyl-2-(diphenylmethylidene)hydrazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1-Tert-butyl-2-(diphenylmethylidene)hydrazine

Chemical Property:

Vapor Pressure:1.81E-05mmHg at 25°C
Boiling Point:363.4°Cat760mmHg
Flash Point:173.6°C
Density:0.96g/cm³
XLogP3:4.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:252.162648646
Heavy Atom Count:19
Complexity:269

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)NN=C(C1=CC=CC=C1)C2=CC=CC=C2

Technology Process of 1-Tert-butyl-2-(diphenylmethylidene)hydrazine

There total 6 articles about 1-Tert-butyl-2-(diphenylmethylidene)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 32818-95-4
N-benzylidene-N'-tert-butylhydrazine

: 24398-53-6
benzophenone-tert-butylhydrazone

Guidance literature:: With sodium t-butanolate; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; bis[2-(diphenylphosphino)phenyl] ether; In 1,4-dioxane; at 80 ℃; for 24h;
DOI:10.1021/ja064782t

Reference yield:

: 100-52-7
benzaldehyde

: 24398-53-6
benzophenone-tert-butylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / acetic acid

2: sodium tert-butoxide / Pd₂(dba)3; bis(2-diphenylphosphinophenyl)ether / dioxane / 24 h / 80 °C

With sodium t-butanolate; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; acetic acid; bis[2-(diphenylphosphino)phenyl] ether; In 1,4-dioxane;
DOI:10.1021/ja064782t