1,1,1,3,3,3-Hexafluoro-2-[2-(2-hydroxy-2,2-diphenyl-ethylselanyl)-phenyl]-propan-2-ol

Base Information

• Chemical Name: 1,1,1,3,3,3-Hexafluoro-2-[2-(2-hydroxy-2,2-diphenyl-ethylselanyl)-phenyl]-propan-2-ol
• CAS No.: 152582-70-2
• Molecular Formula: C₂₃H₁₈F₆O₂Se
• Molecular Weight: 519.345

Synonyms:1,1,1,3,3,3-Hexafluoro-2-[2-(2-hydroxy-2,2-diphenyl-ethylselanyl)-phenyl]-propan-2-ol

Chemical Property of 1,1,1,3,3,3-Hexafluoro-2-[2-(2-hydroxy-2,2-diphenyl-ethylselanyl)-phenyl]-propan-2-ol

Chemical Property:

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Technology Process of 1,1,1,3,3,3-Hexafluoro-2-[2-(2-hydroxy-2,2-diphenyl-ethylselanyl)-phenyl]-propan-2-ol

There total 2 articles about 1,1,1,3,3,3-Hexafluoro-2-[2-(2-hydroxy-2,2-diphenyl-ethylselanyl)-phenyl]-propan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

C23H16F6O2Se (152582-72-4) → phenyl benzyl ketone (451-40-1) + 3,3-Bis-trifluoromethyl-3H-benzo[c][1,2]oxaselenole + 3,3-Bis-trifluoromethyl-3H-benzo[c][1,2]oxaselenole 1-oxide + 1,1,1,3,3,3-Hexafluoro-2-[2-(2-hydroxy-2,2-diphenyl-ethylselanyl)-phenyl]-propan-2-ol (152582-70-2) + (4,4-Bis-trifluoromethyl-4H-3-oxa-1-selena-naphthalen-2-yl)-diphenyl-methanol + C18H10F12O2Se2

Guidance literature:

In ⁽²⁾H₈-toluene; at 150 ℃; for 48h; also dibenzyl 1,2-oxaselenetane (5b);

DOI:10.1021/ja00075a099

Reference yield:

benzophenone (119-61-9) + lithium 1,1,1,3,3,3-hexafluoro-2-(2-lithiophenyl)-2-propoxide (70091-67-7) + tri-n-butylstannylmethyl iodide (66222-29-5) → 1,1,1,3,3,3-Hexafluoro-2-[2-(2-hydroxy-2,2-diphenyl-ethylselanyl)-phenyl]-propan-2-ol (152582-70-2)

Guidance literature:

With selenium; n-butyllithium; Yield given. Multistep reaction;

DOI:10.1021/ja00075a099

Reference yield: 100.0%

1,1,1,3,3,3-Hexafluoro-2-[2-(2-hydroxy-2,2-diphenyl-ethylselanyl)-phenyl]-propan-2-ol (152582-70-2) → C23H16F6O2Se (152582-72-4)

Guidance literature:

With bromine; triethylamine; In tetrachloromethane; at 25 ℃; for 3h;

DOI:10.1021/ja00075a099

upstream raw materials:

benzophenone

lithium 1,1,1,3,3,3-hexafluoro-2-(2-lithiophenyl)-2-propoxide

tri-n-butylstannylmethyl iodide

C₂₃H₁₆F₆O₂Se

Downstream raw materials:

C₂₃H₁₆F₆O₂Se

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