Zirconium oxide dichloride

Base Information

• Chemical Name: Zirconium oxide dichloride
• CAS No.: 7699-43-6
• Molecular Formula: Cl₂OZr
• Molecular Weight: 178.129
• Hs Code.: 2827491000
• UNII: T4294601O7
• Mol file: 7699-43-6.mol

Synonyms:ZC;Zirconium chloride oxide (ZrCl2O);Zirconium chloride oxide(ZrOCl2);Zirconium dichloride monoxide;Zirconiumdichloride oxide;Zirconium dichloride oxide (ZrCl2O);Zirconium oxide dichloride;Zirconium oxychloride;Zirconium oxydichloride;Zirconium(IV) oxychloride;Zirconyl chloride;Zirconyl dichloride;ZircosolZC;Zircosol ZC 20;Basiczirconium chloride;NSC 115914;Oxozirconium(IV)chloride;

Chemical Property of Zirconium oxide dichloride

Chemical Property:

• Appearance/Colour: White or yellow silky odorless crystals
• Melting Point: -15 °C
• PSA: 17.07000
• Density: 1.344 g/mL at 25 °C
• LogP: 1.26020
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 0
• Exact Mass: 175.837319
• Heavy Atom Count: 4
• Complexity: 0

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s): C
• Hazard Codes: C:Corrosive
• Statements: R23:; R34:
• Safety Statements: S26:; S36:; S45:

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: [O-2].[Cl-].[Cl-].[Zr+4]

Technology Process of Zirconium oxide dichloride

There total 18 articles about Zirconium oxide dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

carbon dioxide (124-38-9,18923-20-1) + tetra-allylzirconium → zirconyl chloride (7699-43-6) + but-3-enoic acid (625-38-7) + 4-hydroxy-4-(2-propenyl)-hepta-1,6-diene (10202-75-2)

Guidance literature:

With hydrogenchloride; In diethyl ether; CO2 was bubbled through a cold (-78°C) soln. of compound in ether in the absence of light for 3-4 h, aq. HCl was added;;

DOI:10.1016/S0020-1693(00)82445-7

Reference yield: 50.0%

carbon dioxide (124-38-9,18923-20-1) + tetrabenzylzirconium(IV) (24356-01-2) → phenylacetic acid (103-82-2) + zirconyl chloride (7699-43-6) + tribenzylcarbinol (6712-97-6)

Guidance literature:

With hydrogenchloride; In diethyl ether; CO2 was bubbled through a cold (-78°C) soln. of compound in ether in the absence of light for 3-4 h, aq. HCl was added;;

DOI:10.1016/S0020-1693(00)82445-7

Reference yield:

thionyl chloride (7719-09-7) + zirconium(IV) oxide (7440-67-7) → zirconyl chloride (7699-43-6) + zirconium(IV) chloride (10026-11-6)

Guidance literature:

With O₂; In neat (no solvent, gas phase); thermal-sublimation column, dried O2-Ar mixture as carrier gas for SOCl2 (partial pressure: 13 kPa), heating (350 - 375°C, 15 - 120 min); drying the products over P2O5, elem. anal., product ratio depending on deposition temp., not separated;

upstream raw materials:

water

zirconium(IV) chloride

sodium hydroxide

zirconium trichloride

Refernces

Thermal decomposition of several layered zirconium salts

10.1023/A:1010136403670

The study investigates the thermal decomposition of zirconium molybdate, tungstate, and arsenate, focusing on their mass losses and thermal behavior. The chemicals used in the study include zirconium oxychloride, ammonium-heptamolybdate, hydrochloric acid, ammonium-paratungstate, arsenic acid, and conc. hydrochloric acid, which served as starting materials and reagents for the synthesis of the zirconium salts. The purpose of these chemicals was to prepare well-defined crystalline forms of the zirconium salts for thermal analysis, aiming to understand their thermal behavior and decomposition processes.

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