ethyl (1S,2R)-2-{[(benzyloxy)carbonyl]amino}-5-oxocyclohexanecarboxylate

Base Information

Chemical Name:ethyl (1S,2R)-2-{[(benzyloxy)carbonyl]amino}-5-oxocyclohexanecarboxylate
CAS No.:1092728-41-0
Molecular Formula:C₁₇H₂₁NO₅
Molecular Weight:319.357
Hs Code.:

Synonyms:ethyl (1S,2R)-2-{[(benzyloxy)carbonyl]amino}-5-oxocyclohexanecarboxylate

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Chemical Property of ethyl (1S,2R)-2-{[(benzyloxy)carbonyl]amino}-5-oxocyclohexanecarboxylate

Chemical Property:

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Technology Process of ethyl (1S,2R)-2-{[(benzyloxy)carbonyl]amino}-5-oxocyclohexanecarboxylate

There total 5 articles about ethyl (1S,2R)-2-{[(benzyloxy)carbonyl]amino}-5-oxocyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1092728-40-9
ethyl (7S,8R)-8-{[(benzyloxy)carbonyl]amino}-1,4-dioxaspiro[4.5]decane-7-carboxylate

: 1092728-41-0
ethyl (1S,2R)-2-{[(benzyloxy)carbonyl]amino}-5-oxocyclohexanecarboxylate

Guidance literature:: With hydrogenchloride; In water; acetone; at 20 ℃; Cooling with ice;

Reference yield:

: 813445-18-0
ethyl (R)-8-((1-phenylethyl)amino)-1,4-dioxaspiro[4.5]dec-7-ene-7-carboxylate

: 1092728-41-0
ethyl (1S,2R)-2-{[(benzyloxy)carbonyl]amino}-5-oxocyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium tetrahydroborate / isobutyric Acid / 0 - 20 °C

1.2: 2 h / 0 - 10 °C

2.1: hydrogen / palladium 10% on activated carbon / ethanol; water / 5 h / 50 °C / Inert atmosphere

3.1: sodium carbonate / water; tetrahydrofuran / 20 °C / Cooling with ice

4.1: hydrogenchloride / water; acetone / 20 °C / Cooling with ice

With hydrogenchloride; sodium tetrahydroborate; hydrogen; sodium carbonate; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; water; acetone; isobutyric Acid;

Reference yield:

: 121210-56-8
ethyl 8-hydroxy-1,4-dioxaspiro[4.5]dec-7-ene-7-carboxylate

: 1092728-41-0
ethyl (1S,2R)-2-{[(benzyloxy)carbonyl]amino}-5-oxocyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 5 steps

1.1: toluene-4-sulfonic acid / toluene / 17 h / 70 °C / Reflux

2.1: sodium tetrahydroborate / isobutyric Acid / 0 - 20 °C

2.2: 2 h / 0 - 10 °C

3.1: hydrogen / palladium 10% on activated carbon / ethanol; water / 5 h / 50 °C / Inert atmosphere

4.1: sodium carbonate / water; tetrahydrofuran / 20 °C / Cooling with ice

5.1: hydrogenchloride / water; acetone / 20 °C / Cooling with ice

With hydrogenchloride; sodium tetrahydroborate; hydrogen; sodium carbonate; toluene-4-sulfonic acid; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; water; acetone; toluene; isobutyric Acid;