Technology Process of N-(4-methylphenylmethyl)xanthone imine
There total 1 articles about N-(4-methylphenylmethyl)xanthone imine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
titanium tetrachloride;
In
toluene;
at 0 ℃;
Inert atmosphere;
Reflux;
DOI:10.1021/ol802070d
- Guidance literature:
-
N-(4-methylphenylmethyl)xanthone imine; chlorobenzene;
With
bis(η3-allyl-μ-chloropalladium(II)); cesiumhydroxide monohydrate; tricyclohexylphosphine;
In
5,5-dimethyl-1,3-cyclohexadiene;
for 24h;
Reflux;
Inert atmosphere;
With
hydrogenchloride; sodium cyanoborohydride;
In
ethanol; water;
at 25 ℃;
for 2h;
With
hydrogenchloride;
In
ethanol; water;
at 25 ℃;
for 2h;
DOI:10.1016/j.tet.2009.02.034
- Guidance literature:
-
N-(4-methylphenylmethyl)xanthone imine; chlorobenzene;
With
cesium hydroxide monohydrate; bis(η3-allyl-μ-chloropalladium(II)); tricyclohexylphosphine;
In
toluene;
for 24h;
Inert atmosphere;
Reflux;
With
hydrogenchloride; sodium cyanoborohydride;
In
ethanol;
at 25 ℃;
for 2h;
Inert atmosphere;
DOI:10.1021/ol802070d
