4?benzyloxy pyridine?2,6?dicarboxylic acid dihydrazide

Base Information

Chemical Name:4?benzyloxy pyridine?2,6?dicarboxylic acid dihydrazide
CAS No.:18986-24-8
Molecular Formula:C₁₄H₁₅N₅O₃
Molecular Weight:301.305
Hs Code.:

Synonyms:4?benzyloxy pyridine?2,6?dicarboxylic acid dihydrazide

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Chemical Property of 4?benzyloxy pyridine?2,6?dicarboxylic acid dihydrazide

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Technology Process of 4?benzyloxy pyridine?2,6?dicarboxylic acid dihydrazide

There total 5 articles about 4?benzyloxy pyridine?2,6?dicarboxylic acid dihydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.6%

: 18986-14-6
4?benzyloxy pyridine?2,6?dicarboxylic acid diethyl ester

: 18986-24-8
4?benzyloxy pyridine?2,6?dicarboxylic acid dihydrazide

Guidance literature:: With hydrazine hydrate; In ethanol; for 2h; Reflux;
DOI:10.1007/s12149-019-01341-0

Reference yield:

: 100-39-0
benzyl bromide

: 18986-24-8
4?benzyloxy pyridine?2,6?dicarboxylic acid dihydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / K₂CO₃ / dimethylformamide / 4 h / 85 °C

2: 92 percent / hydrazine hydrate / ethanol / 12 h / Heating

With potassium carbonate; hydrazine hydrate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1002/chem.200390122

Reference yield:

: 115231-56-6
4-oxo-1,4-dihydropyridine-2,6-diethylcarboxylate

: 18986-24-8
4?benzyloxy pyridine?2,6?dicarboxylic acid dihydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / K₂CO₃ / dimethylformamide / 4 h / 85 °C

2: 92 percent / hydrazine hydrate / ethanol / 12 h / Heating

With potassium carbonate; hydrazine hydrate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1002/chem.200390122