Technology Process of 4?benzyloxy?2,6?dicarboethoxyamino pyridine
There total 7 articles about 4?benzyloxy?2,6?dicarboethoxyamino pyridine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 92 percent / hydrazine hydrate / ethanol / 12 h / Heating
2: aq. HCl; NaNO2 / 0.33 h / 0 °C
3: 12 h / Heating
With
hydrogenchloride; hydrazine hydrate; sodium nitrite;
In
ethanol;
3: Curtius rearrangement;
DOI:10.1002/chem.200390122
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 77 percent / K2CO3 / dimethylformamide / 4 h / 85 °C
2: 92 percent / hydrazine hydrate / ethanol / 12 h / Heating
3: aq. HCl; NaNO2 / 0.33 h / 0 °C
4: 12 h / Heating
With
hydrogenchloride; potassium carbonate; hydrazine hydrate; sodium nitrite;
In
ethanol; N,N-dimethyl-formamide;
4: Curtius rearrangement;
DOI:10.1002/chem.200390122
- Guidance literature:
-
Multi-step reaction with 2 steps
1: aq. HCl; NaNO2 / 0.33 h / 0 °C
2: 12 h / Heating
With
hydrogenchloride; sodium nitrite;
2: Curtius rearrangement;
DOI:10.1002/chem.200390122
