2-[(2-chloroethyl)-2-[[(2-hydroxyethyl)amino]carbonyl]-4,6-dinitroanilino]ethyl methanesulfonate

Base Information

Chemical Name:2-[(2-chloroethyl)-2-[[(2-hydroxyethyl)amino]carbonyl]-4,6-dinitroanilino]ethyl methanesulfonate
CAS No.:851627-43-5
Molecular Formula:C₁₄H₁₉ClN₄O₉S
Molecular Weight:454.845
Hs Code.:

Synonyms:2-[(2-chloroethyl)-2-[[(2-hydroxyethyl)amino]carbonyl]-4,6-dinitroanilino]ethyl methanesulfonate

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Chemical Property of 2-[(2-chloroethyl)-2-[[(2-hydroxyethyl)amino]carbonyl]-4,6-dinitroanilino]ethyl methanesulfonate

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Technology Process of 2-[(2-chloroethyl)-2-[[(2-hydroxyethyl)amino]carbonyl]-4,6-dinitroanilino]ethyl methanesulfonate

There total 8 articles about 2-[(2-chloroethyl)-2-[[(2-hydroxyethyl)amino]carbonyl]-4,6-dinitroanilino]ethyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 680199-31-9
((2-((2-hydroxyethyl)carbamoyl)-4,6-dinitrophenyl)azanediyl)bis(ethane-2,1-diyl)dimethane-sulfonate

: 851627-43-5
2-[(2-chloroethyl)-2-[[(2-hydroxyethyl)amino]carbonyl]-4,6-dinitroanilino]ethyl methanesulfonate

: 2-[bis(2-chloroethyl)amino]-N-(2-hydroxyethyl)-3,5-dinitrobenzamide

Guidance literature:: With lithium chloride; In DMF (N,N-dimethyl-formamide); at 60 ℃; for 2h; Product distribution / selectivity;

Reference yield: 32.0%

: 2386-52-9
silver methanesulfonate

: 851627-43-5
2-[(2-chloroethyl)-2-[[(2-hydroxyethyl)amino]carbonyl]-4,6-dinitroanilino]ethyl methanesulfonate

: 680199-31-9
((2-((2-hydroxyethyl)carbamoyl)-4,6-dinitrophenyl)azanediyl)bis(ethane-2,1-diyl)dimethane-sulfonate

Guidance literature:: 2-[bis(2-chloroethyl)amino]-N-(2-hydroxyethyl)-3,5-dinitrobenzamide; With sodium iodide; In 3-methyl-butan-2-one; at 25 - 70 ℃; for 2h;

silver methanesulfonate; In acetonitrile; at 25 ℃; for 1h; Product distribution / selectivity;

Reference yield:

: 1011708-22-7
methanesulfonic acid 2-[(2-chlorocarbonyl-4,6-dinitro-phenyl)-(2-chloro-ethyl)-amino]-ethyl ester

: 141-43-5
ethanolamine

: 851627-43-5
2-[(2-chloroethyl)-2-[[(2-hydroxyethyl)amino]carbonyl]-4,6-dinitroanilino]ethyl methanesulfonate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide; at 0 ℃; for 0.0833333h;
DOI:10.1016/j.tet.2007.04.044