N-(1-phenylethyl)-N'-[(propan-2-yloxy)carbonyl](propan-2-yloxy)carbohydrazide

Base Information

Chemical Name:N-(1-phenylethyl)-N'-[(propan-2-yloxy)carbonyl](propan-2-yloxy)carbohydrazide
CAS No.:1401932-93-1
Molecular Formula:C₁₅H₂₂N₂O₄
Molecular Weight:294.351
Hs Code.:

Synonyms:N-(1-phenylethyl)-N'-[(propan-2-yloxy)carbonyl](propan-2-yloxy)carbohydrazide

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Chemical Property of N-(1-phenylethyl)-N'-[(propan-2-yloxy)carbonyl](propan-2-yloxy)carbohydrazide

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Technology Process of N-(1-phenylethyl)-N'-[(propan-2-yloxy)carbonyl](propan-2-yloxy)carbohydrazide

There total 6 articles about N-(1-phenylethyl)-N'-[(propan-2-yloxy)carbonyl](propan-2-yloxy)carbohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 2446-83-5
di-isopropyl azodicarboxylate

: 100-39-0
benzyl bromide

: 1401932-93-1
N-(1-phenylethyl)-N'-[(propan-2-yloxy)carbonyl](propan-2-yloxy)carbohydrazide

Guidance literature:: With ammonium chloride; zinc; In tetrahydrofuran; water; for 0.5h;
DOI:10.1080/00397911.2013.851245

Reference yield: 81.0%

: 2446-83-5
di-isopropyl azodicarboxylate

: 108-88-3,15644-74-3,16713-13-6
toluene

: 1401932-93-1
N-(1-phenylethyl)-N'-[(propan-2-yloxy)carbonyl](propan-2-yloxy)carbohydrazide

Guidance literature:: With copper(I) oxide; 1,10-Phenanthroline; di-tert-butyl peroxide; at 110 ℃; for 28h; Reagent/catalyst; Mechanism; Molecular sieve; Inert atmosphere; Schlenk technique; Sealed tube;
DOI:10.1039/c7nj04880g

Reference yield:

: 67-56-1
methanol

: 2446-83-5
di-isopropyl azodicarboxylate

: 25870-62-6
1-phenyl-2-hexanone

: 624-24-8
methyl valerate

: 1401932-93-1
N-(1-phenylethyl)-N'-[(propan-2-yloxy)carbonyl](propan-2-yloxy)carbohydrazide

Guidance literature:: di-isopropyl azodicarboxylate; 1-phenyl-2-hexanone; With cerium(IV) trifluoromethanesulfonate; trimethylsilyl cyanide; 9,10-diphenylanthracene; tetrabutyl-ammonium chloride; titanium tetrachloride; In acetonitrile; at 0 - 50 ℃; for 48h; Inert atmosphere; Irradiation; Glovebox;

methanol; With triethylamine; In acetonitrile; at 20 ℃; for 2h; Inert atmosphere; Glovebox;
DOI:10.1016/j.chempr.2019.11.009