(S)-N-[3-[3-fluoro-4-(N-t-butoxycarbonyl)methylaminophenyl]-2-oxo-5-oxazolidinyl]methylamine

Base Information

Chemical Name:(S)-N-[3-[3-fluoro-4-(N-t-butoxycarbonyl)methylaminophenyl]-2-oxo-5-oxazolidinyl]methylamine
CAS No.:797759-33-2
Molecular Formula:C₁₆H₂₂FN₃O₄
Molecular Weight:339.367
Hs Code.:

Synonyms:(S)-N-[3-[3-fluoro-4-(N-t-butoxycarbonyl)methylaminophenyl]-2-oxo-5-oxazolidinyl]methylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-N-[3-[3-fluoro-4-(N-t-butoxycarbonyl)methylaminophenyl]-2-oxo-5-oxazolidinyl]methylamine

Chemical Property:

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Technology Process of (S)-N-[3-[3-fluoro-4-(N-t-butoxycarbonyl)methylaminophenyl]-2-oxo-5-oxazolidinyl]methylamine

There total 8 articles about (S)-N-[3-[3-fluoro-4-(N-t-butoxycarbonyl)methylaminophenyl]-2-oxo-5-oxazolidinyl]methylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₂₀FN₅O₄

: 797759-33-2
(S)-N-[3-[3-fluoro-4-(N-t-butoxycarbonyl)methylaminophenyl]-2-oxo-5-oxazolidinyl]methylamine

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In methanol; at 20 ℃; for 12h; under 2585.81 Torr;

Reference yield:

: tert-butyl (2-fluoro-4-nitrophenyl)(methyl)carbamate

: 797759-33-2
(S)-N-[3-[3-fluoro-4-(N-t-butoxycarbonyl)methylaminophenyl]-2-oxo-5-oxazolidinyl]methylamine

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogen / palladium 10% on activated carbon / methanol / 12 h / 20 °C / 2585.81 Torr

2.1: sodium hydrogencarbonate / water; acetone / 14 h / 20 °C

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -70 °C

3.2: 14 h / -70 - 20 °C

4.1: triethylamine / dichloromethane / 6 h / 20 °C

5.1: sodium azide / DMF (N,N-dimethyl-formamide) / 6 h / 20 - 80 °C

6.1: hydrogen / palladium 10% on activated carbon / methanol / 12 h / 20 °C / 2585.81 Torr

With n-butyllithium; sodium azide; hydrogen; sodium hydrogencarbonate; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; methanol; DMF (N,N-dimethyl-formamide); hexane; dichloromethane; water; acetone;

Reference yield:

: tert-butyl (4-amino-2-fluorophenyl)(methyl)carbamate

: 797759-33-2
(S)-N-[3-[3-fluoro-4-(N-t-butoxycarbonyl)methylaminophenyl]-2-oxo-5-oxazolidinyl]methylamine

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydrogencarbonate / water; acetone / 14 h / 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -70 °C

2.2: 14 h / -70 - 20 °C

3.1: triethylamine / dichloromethane / 6 h / 20 °C

4.1: sodium azide / DMF (N,N-dimethyl-formamide) / 6 h / 20 - 80 °C

5.1: hydrogen / palladium 10% on activated carbon / methanol / 12 h / 20 °C / 2585.81 Torr

With n-butyllithium; sodium azide; hydrogen; sodium hydrogencarbonate; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; methanol; DMF (N,N-dimethyl-formamide); hexane; dichloromethane; water; acetone;