3,3-bis[4-[3-(N,N-dimethylamino)propyN-1-yl]phenyl]allyl alcohol

Base Information

Chemical Name:3,3-bis[4-[3-(N,N-dimethylamino)propyN-1-yl]phenyl]allyl alcohol
CAS No.:869015-23-6
Molecular Formula:C₂₅H₂₈N₂O
Molecular Weight:372.51
Hs Code.:

Synonyms:3,3-bis[4-[3-(N,N-dimethylamino)propyN-1-yl]phenyl]allyl alcohol

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Chemical Property of 3,3-bis[4-[3-(N,N-dimethylamino)propyN-1-yl]phenyl]allyl alcohol

Chemical Property:

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Technology Process of 3,3-bis[4-[3-(N,N-dimethylamino)propyN-1-yl]phenyl]allyl alcohol

There total 5 articles about 3,3-bis[4-[3-(N,N-dimethylamino)propyN-1-yl]phenyl]allyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 869015-22-5
3,3-bis(4-ethynylphenyl)allyl alcohol

: 124-40-3
dimethyl amine

: 869015-23-6
3,3-bis[4-[3-(N,N-dimethylamino)propyN-1-yl]phenyl]allyl alcohol

Guidance literature:: copper(l) iodide; In 1,4-dioxane; water; for 1h; Reflux;

Reference yield:

: 5630-56-8
4,4'-diiodobenzophenone

: 869015-23-6
3,3-bis[4-[3-(N,N-dimethylamino)propyN-1-yl]phenyl]allyl alcohol

Guidance literature:: Multi-step reaction with 4 steps

1.1: magnesium; ethylene dibromide / tetrahydrofuran / 0.5 h

1.2: 0.5 h / Reflux

1.3: 0.5 h

2.1: triethylamine / tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / 1.5 h / Inert atmosphere

3.1: potassium carbonate; methanol / 2 h / Inert atmosphere; Cooling with ice-water

4.1: copper(l) iodide / 1,4-dioxane; water / 1 h / Reflux

With methanol; potassium carbonate; magnesium; ethylene dibromide; triethylamine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; water;

Reference yield:

: 673479-16-8
ethyl 3,3-bis-(4-iodophenyl)-acrylate

: 869015-23-6
3,3-bis[4-[3-(N,N-dimethylamino)propyN-1-yl]phenyl]allyl alcohol

Guidance literature:: Multi-step reaction with 4 steps

1: diisobutylaluminium hydride / tetrahydrofuran / 48 h / -10 - 20 °C / Inert atmosphere

2: triethylamine / tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / 1.5 h / Inert atmosphere

3: potassium carbonate; methanol / 2 h / Inert atmosphere; Cooling with ice-water

4: copper(l) iodide / 1,4-dioxane; water / 1 h / Reflux

With methanol; diisobutylaluminium hydride; potassium carbonate; triethylamine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; water;