bis(2,4-dimethoxybenzyl) 4-(3,6-bis((4,5-dimethoxy-2-nitrobenzyl)oxy)-2,7-difluoro-9H-xanthen-9-yl)isophthalate

Base Information

Chemical Name:bis(2,4-dimethoxybenzyl) 4-(3,6-bis((4,5-dimethoxy-2-nitrobenzyl)oxy)-2,7-difluoro-9H-xanthen-9-yl)isophthalate
CAS No.:1352809-13-2
Molecular Formula:C₅₇H₅₀F₂N₂O₁₉
Molecular Weight:1105.02
Hs Code.:

Synonyms:bis(2,4-dimethoxybenzyl) 4-(3,6-bis((4,5-dimethoxy-2-nitrobenzyl)oxy)-2,7-difluoro-9H-xanthen-9-yl)isophthalate

Suppliers and Price of bis(2,4-dimethoxybenzyl) 4-(3,6-bis((4,5-dimethoxy-2-nitrobenzyl)oxy)-2,7-difluoro-9H-xanthen-9-yl)isophthalate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of bis(2,4-dimethoxybenzyl) 4-(3,6-bis((4,5-dimethoxy-2-nitrobenzyl)oxy)-2,7-difluoro-9H-xanthen-9-yl)isophthalate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of bis(2,4-dimethoxybenzyl) 4-(3,6-bis((4,5-dimethoxy-2-nitrobenzyl)oxy)-2,7-difluoro-9H-xanthen-9-yl)isophthalate

There total 5 articles about bis(2,4-dimethoxybenzyl) 4-(3,6-bis((4,5-dimethoxy-2-nitrobenzyl)oxy)-2,7-difluoro-9H-xanthen-9-yl)isophthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1352809-12-1
bis(2,4-dimethoxybenzyl) 4-(2,7-difluoro-3,6-dihydroxy-9H-xanthen-9-yl)isophthalate

: 53413-67-5
6-nitroveratrylbromide

: 1352809-13-2
bis(2,4-dimethoxybenzyl) 4-(3,6-bis((4,5-dimethoxy-2-nitrobenzyl)oxy)-2,7-difluoro-9H-xanthen-9-yl)isophthalate

Guidance literature:: With tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; In dichloromethane; water; at 20 ℃; for 18h; Darkness;
DOI:10.1002/anie.201104571

Reference yield:

: 1352809-16-5
C₂₅H₁₆F₂O₉

: 1352809-13-2
bis(2,4-dimethoxybenzyl) 4-(3,6-bis((4,5-dimethoxy-2-nitrobenzyl)oxy)-2,7-difluoro-9H-xanthen-9-yl)isophthalate

Guidance literature:: Multi-step reaction with 3 steps

1: diisopropyl-carbodiimide / dichloromethane / 18 h / 20 °C

2: ammonium bicarbonate / tetrahydrofuran; methanol; water / 24 h / 20 °C / Darkness

3: tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate / dichloromethane; water / 18 h / 20 °C / Darkness

With tetra(n-butyl)ammonium hydrogensulfate; ammonium bicarbonate; potassium carbonate; diisopropyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1002/anie.201104571

Reference yield:

: 7314-44-5
2,4-dimethoxylbenzyl alcohol

: 1352809-13-2
bis(2,4-dimethoxybenzyl) 4-(3,6-bis((4,5-dimethoxy-2-nitrobenzyl)oxy)-2,7-difluoro-9H-xanthen-9-yl)isophthalate

Guidance literature:: Multi-step reaction with 3 steps

1: diisopropyl-carbodiimide / dichloromethane / 18 h / 20 °C

2: ammonium bicarbonate / tetrahydrofuran; methanol; water / 24 h / 20 °C / Darkness

3: tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate / dichloromethane; water / 18 h / 20 °C / Darkness

With tetra(n-butyl)ammonium hydrogensulfate; ammonium bicarbonate; potassium carbonate; diisopropyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1002/anie.201104571