tris(2-methoxyphenyl)bismuth diacetate

Base Information

Chemical Name:tris(2-methoxyphenyl)bismuth diacetate
CAS No.:185509-57-3
Molecular Formula:C₂₅H₂₇BiO₇
Molecular Weight:648.466
Hs Code.:

Synonyms:tris(2-methoxyphenyl)bismuth diacetate

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Chemical Property of tris(2-methoxyphenyl)bismuth diacetate

Chemical Property:

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Technology Process of tris(2-methoxyphenyl)bismuth diacetate

There total 4 articles about tris(2-methoxyphenyl)bismuth diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: (CH₃OC₆H₄)3BiC(CO₂CH₃)C(CO₂CH₃)NCOC₆H₃(CF₃)2

: 64-19-7,77671-22-8
acetic acid

: 185509-57-3
tris(2-methoxyphenyl)bismuth diacetate

Guidance literature:: In dichloromethane; byproducts: CH3OC(O)CHC(C(O)OCH3)NHC(O)C6H3(CF3)2; acetic acid added to CH2Cl2 soln. of Bi compd. (molar ratio 2.2:1); stirred for 4 h at room temp.; evapd.; sepd. by chromy. (silica gel); E and Z isomers of dimethyl 2-(N-(3,5-bis(trifluoromethyl)benzoyl))aminofumarate (20:80) sepd.; detd. by(1)H NMR;
DOI:10.1016/S0022-328X(00)00295-3

Reference yield: 98.0%

: 233257-04-0
[(trifluoroacetyl)imino]tris(2-methoxyphenyl)-λ5-bismuthane

: 64-19-7,77671-22-8
acetic acid

: 185509-57-3
tris(2-methoxyphenyl)bismuth diacetate

Guidance literature:: In diethyl ether; under Ar; a mixt. of the bismuthane, acetic acid and diethyl ether was stirred at 25°C for 4 h; the mixt. was evapd. under vac., the oily residue was extd. with diethylether, the diethyl ether extract was dried over MgSO4 and evapd. under vac., the oily residue was recrystd. from CH2Cl2/hexane;
DOI:10.1021/ja003623l

Reference yield:

: 121899-81-8
tris(2-methoxyphenyl)bismuth dichloride

: 185509-57-3
tris(2-methoxyphenyl)bismuth diacetate

Guidance literature:: Multi-step reaction with 3 steps

1: KO-t-Bu / dichloromethane

2: dichloromethane

3: dichloromethane

With KO-t-Bu; In dichloromethane;
DOI:10.1016/S0022-328X(00)00295-3