α-(Trimethylsiloxy)-α-<3-(trimethylsiloxy)-3-cyclohexen-1-yl>benzolacetonitril

Base Information

Chemical Name:α-(Trimethylsiloxy)-α-<3-(trimethylsiloxy)-3-cyclohexen-1-yl>benzolacetonitril
CAS No.:73593-62-1
Molecular Formula:C₂₀H₃₁NO₂Si₂
Molecular Weight:373.643
Hs Code.:

Synonyms:α-(Trimethylsiloxy)-α-<3-(trimethylsiloxy)-3-cyclohexen-1-yl>benzolacetonitril

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Chemical Property of α-(Trimethylsiloxy)-α-<3-(trimethylsiloxy)-3-cyclohexen-1-yl>benzolacetonitril

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Technology Process of α-(Trimethylsiloxy)-α-<3-(trimethylsiloxy)-3-cyclohexen-1-yl>benzolacetonitril

There total 4 articles about α-(Trimethylsiloxy)-α-<3-(trimethylsiloxy)-3-cyclohexen-1-yl>benzolacetonitril which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 75-77-4
chloro-trimethyl-silane

: 73593-47-2
α-(3-Oxocyclohexyl)-α-(trimethylsiloxy)benzolacetonitril

: 73593-62-1
α-(Trimethylsiloxy)-α-<3-(trimethylsiloxy)-3-cyclohexen-1-yl>benzolacetonitril

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; 1) -78 degC, 1 h, 2) 0 degC, 2 h;

Reference yield:

: 930-68-7
cyclohexenone

: 73593-62-1
α-(Trimethylsiloxy)-α-<3-(trimethylsiloxy)-3-cyclohexen-1-yl>benzolacetonitril

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / -78 degC -> 0 degC

2: 86 percent / 1) LDA / tetrahydrofuran / 1) -78 degC, 1 h, 2) 0 degC, 2 h

With lithium diisopropyl amide; In tetrahydrofuran; diethyl ether;

Reference yield:

: 25438-37-3
phenyl(trimethylsiloxy)acetonitrile

: 73593-62-1
α-(Trimethylsiloxy)-α-<3-(trimethylsiloxy)-3-cyclohexen-1-yl>benzolacetonitril

Guidance literature:: Multi-step reaction with 3 steps

1: LDA / diethyl ether / -78 °C

2: diethyl ether / -78 degC -> 0 degC

3: 86 percent / 1) LDA / tetrahydrofuran / 1) -78 degC, 1 h, 2) 0 degC, 2 h

With lithium diisopropyl amide; In tetrahydrofuran; diethyl ether;