5-chloro-2-(2-trifluoromethylphenyl)pentanimidic acid ethyl ester hydrochloride

Base Information

Chemical Name:5-chloro-2-(2-trifluoromethylphenyl)pentanimidic acid ethyl ester hydrochloride
CAS No.:1123197-78-3
Molecular Formula:C₁₄H₁₇ClF₃NO*ClH
Molecular Weight:344.204
Hs Code.:

Synonyms:5-chloro-2-(2-trifluoromethylphenyl)pentanimidic acid ethyl ester hydrochloride

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Chemical Property of 5-chloro-2-(2-trifluoromethylphenyl)pentanimidic acid ethyl ester hydrochloride

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Technology Process of 5-chloro-2-(2-trifluoromethylphenyl)pentanimidic acid ethyl ester hydrochloride

There total 3 articles about 5-chloro-2-(2-trifluoromethylphenyl)pentanimidic acid ethyl ester hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.6%

: 64-17-5
ethanol

: 5-chloro-2-(2-(trifluoromethyl)phenyl)pentanenitrile

: 1123197-78-3
5-chloro-2-(2-trifluoromethylphenyl)pentanimidic acid ethyl ester hydrochloride

Guidance literature:: With acetyl chloride; at 0 - 20 ℃; Inert atmosphere;

Reference yield: 81.6%

: 1634-04-4
tert-butyl methyl ether

: 75-36-5
acetyl chloride

: 5-chloro-2-(2-(trifluoromethyl)phenyl)pentanenitrile

: 1123197-78-3
5-chloro-2-(2-trifluoromethylphenyl)pentanimidic acid ethyl ester hydrochloride

Guidance literature:: In ethanol;

Reference yield:

: 3038-47-9
2-(trifluoromethyl)phenylacetonitrile

: 1123197-78-3
5-chloro-2-(2-trifluoromethylphenyl)pentanimidic acid ethyl ester hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butylate / tetrahydrofuran / 0.17 h / -10 °C / Inert atmosphere

1.2: 2 h / 0 - 20 °C

2.1: acetyl chloride / 72 h / 0 - 20 °C / Inert atmosphere

With potassium tert-butylate; acetyl chloride; In tetrahydrofuran;