(S)-2-Benzyloxycarbonylamino-6-(hexadecanoyl-hydroxy-amino)-hexanoic acid methyl ester

Base Information

• Chemical Name: (S)-2-Benzyloxycarbonylamino-6-(hexadecanoyl-hydroxy-amino)-hexanoic acid methyl ester
• CAS No.: 171287-53-9
• Molecular Formula: C₃₁H₅₂N₂O₆
• Molecular Weight: 548.764

Synonyms:(S)-2-Benzyloxycarbonylamino-6-(hexadecanoyl-hydroxy-amino)-hexanoic acid methyl ester

Chemical Property of (S)-2-Benzyloxycarbonylamino-6-(hexadecanoyl-hydroxy-amino)-hexanoic acid methyl ester

Chemical Property:

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Technology Process of (S)-2-Benzyloxycarbonylamino-6-(hexadecanoyl-hydroxy-amino)-hexanoic acid methyl ester

There total 9 articles about (S)-2-Benzyloxycarbonylamino-6-(hexadecanoyl-hydroxy-amino)-hexanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

(S)-2-Benzyloxycarbonylamino-6-hydroxyamino-hexanoic acid methyl ester (157505-72-1) + n-hexadecanoyl chloride (112-67-4) → (S)-2-Benzyloxycarbonylamino-6-(hexadecanoyl-hydroxy-amino)-hexanoic acid methyl ester (171287-53-9)

Guidance literature:

With sodium hydrogencarbonate; In dichloromethane; for 3h; Ambient temperature;

DOI:10.1021/ja963968x

Reference yield:

C18H26N2O5 (157505-71-0) → (S)-2-Benzyloxycarbonylamino-6-(hexadecanoyl-hydroxy-amino)-hexanoic acid methyl ester (171287-53-9)

Guidance literature:

Multi-step reaction with 2 steps

1: NH₂OH*HCl / methanol / 0.17 h / 40 °C

2: 71 percent / NaHCO₃ / CH₂Cl₂ / 3 h / Ambient temperature

With hydroxylamine hydrochloride; sodium hydrogencarbonate; In methanol; dichloromethane;

DOI:10.1021/ja963968x

Reference yield:

C47H82N2O7 (945496-81-1) → (S)-2-Benzyloxycarbonylamino-6-(hexadecanoyl-hydroxy-amino)-hexanoic acid methyl ester (171287-53-9)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In methanol;

DOI:10.1039/b703116e

upstream raw materials:

(S)-2-Benzyloxycarbonylamino-6-hydroxyamino-hexanoic acid methyl ester

n-hexadecanoyl chloride

C₄₇H₈₂N₂O₇

C₂₁H₂₄N₂O₅

Downstream raw materials:

[(S)-1-[(S)-1-(tert-Butyl-diphenyl-silanyloxy)-2-oxo-azepan-3-ylcarbamoyl]-2-((S)-6-(hexadecanoyl-hydroxy-amino)-2-{[(S)-2-(2-hydroxy-phenyl)-4,5-dihydro-oxazole-4-carbonyl]-amino}-hexanoylamino)-ethyl]-carbamic acid tert-butyl ester

(S)-2-(2-Hydroxy-phenyl)-4,5-dihydro-oxazole-4-carboxylic acid [(S)-1-{2-[(S)-1-(tert-butyl-diphenyl-silanyloxy)-2-oxo-azepan-3-ylcarbamoyl]-ethylcarbamoyl}-5-(hexadecanoyl-hydroxy-amino)-pentyl]-amide

(S)-6-[Hexadecanoyl-(2-trimethylsilanyl-ethoxymethoxy)-amino]-2-{[(S)-2-(2-hydroxy-phenyl)-4,5-dihydro-oxazole-4-carbonyl]-amino}-hexanoic acid methyl ester

(S)-6-[Hexadecanoyl-(2-trimethylsilanyl-ethoxymethoxy)-amino]-2-{[(S)-2-(2-hydroxy-phenyl)-4,5-dihydro-oxazole-4-carbonyl]-amino}-hexanoic acid

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