(2R,3R)-2-Benzyl-3-hydroxy-pentanedioic acid 5-ethyl ester

Base Information

Chemical Name:(2R,3R)-2-Benzyl-3-hydroxy-pentanedioic acid 5-ethyl ester
CAS No.:651735-54-5
Molecular Formula:C₁₄H₁₈O₅
Molecular Weight:266.294
Hs Code.:

Synonyms:(2R,3R)-2-Benzyl-3-hydroxy-pentanedioic acid 5-ethyl ester

Suppliers and Price of (2R,3R)-2-Benzyl-3-hydroxy-pentanedioic acid 5-ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2R,3R)-2-Benzyl-3-hydroxy-pentanedioic acid 5-ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2R,3R)-2-Benzyl-3-hydroxy-pentanedioic acid 5-ethyl ester

There total 5 articles about (2R,3R)-2-Benzyl-3-hydroxy-pentanedioic acid 5-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54813-93-3
diethyl 2-benzyl-3-ketoglutarate

: 651735-54-5
(2R,3R)-2-Benzyl-3-hydroxy-pentanedioic acid 5-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 97 percent Chromat_. / glucose; NaCl; NADPH / NADPH-dependent ketoreductase KRED-108; lyophilized glucose dehydrogenase / aq. phosphate buffer; dimethylsulfoxide / 37 °C / pH 6.5 / Enzymatic reaction

2.1: NaOH / ethanol; H₂O / 20 °C

2.2: HCl / ethanol; H₂O / pH 2 - 2.5

3.1: conc. HCl / 45 - 50 °C

With hydrogenchloride; sodium hydroxide; D-glucose; NADPH; sodium chloride; lyophilized glucose dehydrogenase; NADPH-dependent ketoreductase KRED-108; In phosphate buffer; ethanol; water; dimethyl sulfoxide;

Reference yield:

: 100-39-0
benzyl bromide

: 651735-54-5
(2R,3R)-2-Benzyl-3-hydroxy-pentanedioic acid 5-ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium diisopropylamine / hexane; tetrahydrofuran / 0.17 h / -18 °C

1.2: tetrahydrofuran; hexane / 4.5 h / -18 - 20 °C

2.1: 97 percent Chromat_. / glucose; NaCl; NADPH / NADPH-dependent ketoreductase KRED-108; lyophilized glucose dehydrogenase / aq. phosphate buffer; dimethylsulfoxide / 37 °C / pH 6.5 / Enzymatic reaction

3.1: NaOH / ethanol; H₂O / 20 °C

3.2: HCl / ethanol; H₂O / pH 2 - 2.5

4.1: conc. HCl / 45 - 50 °C

With hydrogenchloride; sodium hydroxide; D-glucose; NADPH; sodium chloride; lithium diisopropyl amide; lyophilized glucose dehydrogenase; NADPH-dependent ketoreductase KRED-108; In tetrahydrofuran; phosphate buffer; ethanol; hexane; water; dimethyl sulfoxide;

Reference yield:

: 105-50-0
diethyl 1,3-acetonedicarboxylate

: 651735-54-5
(2R,3R)-2-Benzyl-3-hydroxy-pentanedioic acid 5-ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium diisopropylamine / hexane; tetrahydrofuran / 0.17 h / -18 °C

1.2: tetrahydrofuran; hexane / 4.5 h / -18 - 20 °C

2.1: 97 percent Chromat_. / glucose; NaCl; NADPH / NADPH-dependent ketoreductase KRED-108; lyophilized glucose dehydrogenase / aq. phosphate buffer; dimethylsulfoxide / 37 °C / pH 6.5 / Enzymatic reaction

3.1: NaOH / ethanol; H₂O / 20 °C

3.2: HCl / ethanol; H₂O / pH 2 - 2.5

4.1: conc. HCl / 45 - 50 °C

With hydrogenchloride; sodium hydroxide; D-glucose; NADPH; sodium chloride; lithium diisopropyl amide; lyophilized glucose dehydrogenase; NADPH-dependent ketoreductase KRED-108; In tetrahydrofuran; phosphate buffer; ethanol; hexane; water; dimethyl sulfoxide;