(2E)-N,N,N-trimethyl-3-phenylprop-2-en-1-aminium trifluoromethanesulfonate

Base Information

Chemical Name:(2E)-N,N,N-trimethyl-3-phenylprop-2-en-1-aminium trifluoromethanesulfonate
CAS No.:1421354-42-8
Molecular Formula:CF₃O₃S*C₁₂H₁₈N
Molecular Weight:325.352
Hs Code.:

Synonyms:(2E)-N,N,N-trimethyl-3-phenylprop-2-en-1-aminium trifluoromethanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2E)-N,N,N-trimethyl-3-phenylprop-2-en-1-aminium trifluoromethanesulfonate

Chemical Property:

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Technology Process of (2E)-N,N,N-trimethyl-3-phenylprop-2-en-1-aminium trifluoromethanesulfonate

There total 2 articles about (2E)-N,N,N-trimethyl-3-phenylprop-2-en-1-aminium trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 2926-30-9
sodium triflate

: 4392-24-9
Cinnamyl bromide

: 75-50-3
trimethylamine

: 1421354-42-8
(2E)-N,N,N-trimethyl-3-phenylprop-2-en-1-aminium trifluoromethanesulfonate

Guidance literature:: In ethanol; acetone; at 20 ℃; for 0.5h;
DOI:10.1002/chem.201201772

Reference yield:

: 42817-44-7
(E)-N,N-dimethyl-3-phenylprop-2-en-1-amine

: 333-27-7
methyl trifluoromethanesulfonate

: 1421354-42-8
(2E)-N,N,N-trimethyl-3-phenylprop-2-en-1-aminium trifluoromethanesulfonate

Guidance literature:: In diethyl ether;
DOI:10.1021/jacs.8b08792

Reference yield: 51.0%

: 498-66-8
norbornene

: 1421354-42-8
(2E)-N,N,N-trimethyl-3-phenylprop-2-en-1-aminium trifluoromethanesulfonate

: 5720-07-0
4-methoxyphenylboronic acid

: (1S,2R,3S,4R)-2-cinnamyl-3-(4-methoxyphenyl)bicyclo[2.2.1]heptane

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,4-dioxane; acetonitrile; at 120 ℃; for 2h; stereoselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.joc.1c01339