Technology Process of C24H24ClFN4O
There total 10 articles about C24H24ClFN4O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrogenchloride; sodium nitrite / water / 0.5 h / 0 - 5 °C
1.2: 1 h / 75 °C
2.1: copper diacetate; pyridine / dichloromethane / 16 h / 23 °C
3.1: hydrogenchloride; palladium 10% on activated carbon; hydrogen / methanol / 6 h / 23 °C
4.1: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / 23 °C
With
pyridine; hydrogenchloride; palladium 10% on activated carbon; hydrogen; copper diacetate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium nitrite;
In
methanol; dichloromethane; water;
- Guidance literature:
-
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
at 23 ℃;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: hydrazine hydrate / ethanol / 3 h / Reflux
2.1: hydrogenchloride; sodium nitrite / water / 0.5 h / 0 - 5 °C
2.2: 1 h / 75 °C
3.1: copper diacetate; pyridine / dichloromethane / 16 h / 23 °C
4.1: hydrogenchloride; palladium 10% on activated carbon; hydrogen / methanol / 6 h / 23 °C
5.1: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / 23 °C
With
pyridine; hydrogenchloride; palladium 10% on activated carbon; hydrogen; copper diacetate; benzotriazol-1-ol; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium nitrite;
In
methanol; ethanol; dichloromethane; water;