N,N'-bispyridinecarboxamide-4,5-dimethylbenzenediamine

Base Information

Chemical Name:N,N'-bispyridinecarboxamide-4,5-dimethylbenzenediamine
CAS No.:216389-76-3
Molecular Formula:C₂₀H₁₈N₄O₂
Molecular Weight:346.389
Hs Code.:

Synonyms:N,N'-bispyridinecarboxamide-4,5-dimethylbenzenediamine

Suppliers and Price of N,N'-bispyridinecarboxamide-4,5-dimethylbenzenediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-bispyridinecarboxamide-4,5-dimethylbenzenediamine

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Technology Process of N,N'-bispyridinecarboxamide-4,5-dimethylbenzenediamine

There total 1 articles about N,N'-bispyridinecarboxamide-4,5-dimethylbenzenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 98-98-6
2-Picolinic acid

: 3171-45-7
4,5-dimethyl-1,2-phenylenediamine

: 216389-76-3
N,N'-bispyridinecarboxamide-4,5-dimethylbenzenediamine

Guidance literature:: With triphenyl phosphite; tetrabutylammomium bromide; at 120 ℃; for 1h;
DOI:10.1016/j.poly.2010.04.017

Reference yield: 75.0%

: 14898-67-0
ruthenium(III) chloride trihydrate

: 216389-76-3
N,N'-bispyridinecarboxamide-4,5-dimethylbenzenediamine

: 10102-43-9
nitrogen(II) oxide

: 108-88-3,15644-74-3,16713-13-6
toluene

: [(1,2-bis(pyridine-2-carboxamido)-4,5-dimethylbenzene)-H₂)Ru(NO)(Cl)]*toluene

Guidance literature:: With NaH; In N,N-dimethyl-formamide; byproducts: H2, NaCl; a slurry of NaH in DMF was added to a stirred soln. of pyridine-compoundin DM, RuCl3*3H2O was added, the mixt. was heated to reflux for 20 h un der N2, cooled to room temp., filtered, heated to reflux and NO gas was passed through it for 3 h; concd., diethyl ether was added, ppt. was filtered off, washed with dry diethyl ether, dried under vac.; elem. anal.;
DOI:10.1021/ic040030t