2-(4-methoxybenzylamino)-3-phenypropionic acid methyl ester

Base Information

Chemical Name:2-(4-methoxybenzylamino)-3-phenypropionic acid methyl ester
CAS No.:344765-03-3
Molecular Formula:C₁₈H₂₁NO₃
Molecular Weight:299.37
Hs Code.:

Synonyms:2-(4-methoxybenzylamino)-3-phenypropionic acid methyl ester

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Chemical Property of 2-(4-methoxybenzylamino)-3-phenypropionic acid methyl ester

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Technology Process of 2-(4-methoxybenzylamino)-3-phenypropionic acid methyl ester

There total 10 articles about 2-(4-methoxybenzylamino)-3-phenypropionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 7524-50-7
methyl (2S)-2-amino-3-phenylpropanoate hydrochloride

: 123-11-5
4-methoxy-benzaldehyde

: 344765-03-3
2-(4-methoxybenzylamino)-3-phenypropionic acid methyl ester

Guidance literature:: methyl (2S)-2-amino-3-phenylpropanoate hydrochloride; 4-methoxy-benzaldehyde; With triethylamine; In methanol; at 20 ℃; for 1h;

With sodium tetrahydroborate; In methanol; at 0 - 20 ℃; for 1h;
DOI:10.1080/00397911.2019.1671983

Reference yield: 79.0%

: 1010385-00-8
C₁₉H₂₃NO₃

: 2439-60-3,27442-39-3
N-methyl-L-phenylalanine methyl ester

: 344765-03-3
2-(4-methoxybenzylamino)-3-phenypropionic acid methyl ester

Guidance literature:: C₁₉H₂₃NO₃; With N-iodo-succinimide; In acetonitrile; at 20 ℃;

With N-methoxylamine hydrochloride; In acetonitrile; at 20 ℃; Further stages.;
DOI:10.1016/j.tetlet.2007.11.162

Reference yield:

: 7524-50-7
methyl (2S)-2-amino-3-phenylpropanoate hydrochloride

: 33402-67-4
sodium hydroxy(4-methoxyphenyl)methanesulfonate

: 344765-03-3
2-(4-methoxybenzylamino)-3-phenypropionic acid methyl ester

Guidance literature:: methyl (2S)-2-amino-3-phenylpropanoate hydrochloride; sodium hydroxy(4-methoxyphenyl)methanesulfonate; With sodium cyanoborohydride; In methanol; at 20 ℃; for 20h;

With hydrogenchloride; In diethyl ether; at 0 ℃; for 13h;
DOI:10.1016/j.tetlet.2014.03.046