meso-3,4-diphenyl-2,5-hexanedione

Base Information

• Chemical Name: meso-3,4-diphenyl-2,5-hexanedione
• CAS No.: 69373-33-7
• Molecular Formula: C₁₈H₁₈O₂
• Molecular Weight: 266.34

Synonyms:meso-3,4-diphenyl-2,5-hexanedione

Chemical Property of meso-3,4-diphenyl-2,5-hexanedione

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of meso-3,4-diphenyl-2,5-hexanedione

There total 6 articles about meso-3,4-diphenyl-2,5-hexanedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.6%

1-phenyl-acetone (103-79-7,136675-26-8) → meso-3,4-diphenyl-2,5-hexanedione (69373-33-7)

Guidance literature:

With trans-di-O-tert-butyl hyponitrite; at 90 ℃; for 0.5h;

DOI:10.1021/jo00217a044

Reference yield: 13.0%

1-phenyl-acetone (103-79-7,136675-26-8) → meso-3,4-diphenyl-2,5-hexanedione (69373-33-7) + (3R*,4R*)-3,4-diphenyl-2,5-hexanedione (69373-32-6)

Guidance literature:

With lead dioxide; In benzene; for 1h; Heating;

DOI:10.1021/jo00355a010

Reference yield: 12.0%

4-methoxyphenyllead(IV) triacetate (18649-43-9) + 1-Phenyl-2-propanone Potassium Enolate (57918-71-5) → meso-3,4-diphenyl-2,5-hexanedione (69373-33-7) + (3R*,4R*)-3,4-diphenyl-2,5-hexanedione (69373-32-6) + 1-(4-methoxyphenyl)-1-phenyl-2-propanone (183171-83-7)

Guidance literature:

With pyridine; In tetrahydrofuran; for 1h; Ambient temperature;

DOI:10.1039/a607543f

upstream raw materials:

diacetyl peroxide

1-phenyl-acetone

4-methoxyphenyllead(IV) triacetate

1-Phenyl-2-propanone Potassium Enolate

Downstream raw materials:

N-phenyl-2,5-dimethyl-3,4-diphenylpyrrole

meso-2,3-diphenylsuccinic acid

1-benzyl-3,4,-diphenyl-2,5-dimethylpyrrole

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