3-(4-methoxyphenyl)-2-(4-methylbenzenesulfonyl)-1,2,3,4-tetrahydroisoquinoline

Base Information

Chemical Name:3-(4-methoxyphenyl)-2-(4-methylbenzenesulfonyl)-1,2,3,4-tetrahydroisoquinoline
CAS No.:1182624-46-9
Molecular Formula:C₂₃H₂₃NO₃S
Molecular Weight:393.507
Hs Code.:

Synonyms:3-(4-methoxyphenyl)-2-(4-methylbenzenesulfonyl)-1,2,3,4-tetrahydroisoquinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(4-methoxyphenyl)-2-(4-methylbenzenesulfonyl)-1,2,3,4-tetrahydroisoquinoline

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Technology Process of 3-(4-methoxyphenyl)-2-(4-methylbenzenesulfonyl)-1,2,3,4-tetrahydroisoquinoline

There total 14 articles about 3-(4-methoxyphenyl)-2-(4-methylbenzenesulfonyl)-1,2,3,4-tetrahydroisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 130907-16-3
2-(4-methoxyphenethyl)benzaldehyde

: 70-55-3
toluene-4-sulfonamide

: 1182624-46-9
3-(4-methoxyphenyl)-2-(4-methylbenzenesulfonyl)-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: With scandium tris(trifluoromethanesulfonate); In 1,2-dichloro-ethane; at 20 ℃; Reflux;
DOI:10.1021/ol300180w

Reference yield: 92.0%

: 1363394-64-2
N-(2-(4-methoxyphenethyl)benzylidene)-4-methylbenzenesulfonamide

: 1182624-46-9
3-(4-methoxyphenyl)-2-(4-methylbenzenesulfonyl)-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: With boron trifluoride diethyl etherate; In 1,2-dichloro-ethane; at 50 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jo300635m

Reference yield: 81.0%

: 909792-50-3
methyl [2-{(trimethylsilyl)methyl}phenyl]methyl carbonate

: 14674-38-5
N-(4-methoxybenzylidene)-p-toluenesulfonamide

: 1182624-46-9
3-(4-methoxyphenyl)-2-(4-methylbenzenesulfonyl)-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: With allyl(cyclopentadiene)palladium(II); 1,5-bis-(diphenylphosphino)pentane; In N,N-dimethyl-formamide; at 120 ℃; for 24h;
DOI:10.1021/ja905988e