4-benzyloxyphenylacetaldehyde diethyl acetal

Base Information

Chemical Name:4-benzyloxyphenylacetaldehyde diethyl acetal
CAS No.:1430737-04-4
Molecular Formula:C₁₉H₂₄O₃
Molecular Weight:300.398
Hs Code.:

Synonyms:4-benzyloxyphenylacetaldehyde diethyl acetal

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Chemical Property of 4-benzyloxyphenylacetaldehyde diethyl acetal

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Technology Process of 4-benzyloxyphenylacetaldehyde diethyl acetal

There total 4 articles about 4-benzyloxyphenylacetaldehyde diethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 64-17-5
ethanol

: 40167-10-0
2-[4-(benzyloxy)phenyl]acetaldehyde

: 1430737-04-4
4-benzyloxyphenylacetaldehyde diethyl acetal

Guidance literature:: With sulfuric acid; at 25 ℃; for 3h; Dean-Stark;
DOI:10.1016/j.tet.2013.03.052

Reference yield:

: 61439-59-6
2-(4-benzyloxyphenyl)ethanol

: 1430737-04-4
4-benzyloxyphenylacetaldehyde diethyl acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 2-iodoxybenzoic acid / dimethyl sulfoxide / 3 h / 25 °C

2: sulfuric acid / 3 h / 25 °C / Dean-Stark

With sulfuric acid; 2-iodoxybenzoic acid; In dimethyl sulfoxide;
DOI:10.1016/j.tet.2013.03.052

Reference yield:

: 501-94-0
p-hydroxyphenethyl alcohol

: 1430737-04-4
4-benzyloxyphenylacetaldehyde diethyl acetal

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 25 °C

1.2: 4 h / 25 °C

2.1: 2-iodoxybenzoic acid / dimethyl sulfoxide / 3 h / 25 °C

3.1: sulfuric acid / 3 h / 25 °C / Dean-Stark

With sulfuric acid; 2-iodoxybenzoic acid; potassium carbonate; In dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2013.03.052