diethyl 1,4-dihydro-2,4,6-trimethyl-3,5-pyridinedicarboxylate

Base Information

• Chemical Name: diethyl 1,4-dihydro-2,4,6-trimethyl-3,5-pyridinedicarboxylate
• CAS No.: 1150-55-6
• Molecular Formula: C14H19 N O4
• Molecular Weight: 265.309
• NSC Number: 243815
• UNII: PW7DS4L6F7
• DSSTox Substance ID: DTXSID60921585
• Nikkaji Number: J357.706F
• Wikidata: Q82894521
• Mol file: 1150-55-6.mol

Synonyms:3,5-Pyridinedicarboxylicacid, 2,4,6-trimethyl-, diethyl ester (6CI,8CI,9CI); 2,4,6-Trimethyl-3,5-pyridinedicarboxylicacid diethyl ester; 3,5-(Diethoxycarbonyl)-2,4,6-trimethylpyridine;3,5-(Diethoxycarbonyl0collidine;3,5-Bis(ethoxycarbonyl)-2,4,6-trimethylpyridine; Diethyl2,4,6-trimethyl-3,5-pyridinedicarboxylate; NSC 243815

Chemical Property of diethyl 1,4-dihydro-2,4,6-trimethyl-3,5-pyridinedicarboxylate

Chemical Property:

• Vapor Pressure: 0.000359mmHg at 25°C
• Boiling Point: 318.5°C at 760 mmHg
• Flash Point: 146.4°C
• PSA: 65.49000
• Density: 1.104g/cm³
• LogP: 2.36020
• XLogP3: 2.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 6
• Exact Mass: 265.13140809
• Heavy Atom Count: 19
• Complexity: 301

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCOC(=O)C1=C(C(=C(N=C1C)C)C(=O)OCC)C

Technology Process of diethyl 1,4-dihydro-2,4,6-trimethyl-3,5-pyridinedicarboxylate

There total 6 articles about diethyl 1,4-dihydro-2,4,6-trimethyl-3,5-pyridinedicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethanol (64-17-5) + ethyl acetoacetate (141-97-9) → diethyl 1,4-dihydro-2,4,6-trimethylpyridine-3,5-dicarboxylate (632-93-9) + 2,4,6-trimethylpyridine-3,5-dicarboxylic acid diethyl ester (1150-55-6) + ethyl 2-ethyl-3-oxobutanoate (607-97-6)

Guidance literature:

With sulfur; ammonium bicarbonate; zinc(II) oxide; at 50 ℃; for 24h; Inert atmosphere; Irradiation;

DOI:10.1016/j.jcat.2017.02.029

Reference yield:

ethyl acetoacetate (141-97-9) + benzaldehyde (100-52-7) → 2,4,6-trimethylpyridine-3,5-dicarboxylic acid diethyl ester (1150-55-6) + 2,6-dimethyl-4-phenyl-pyridine-3,5-dicarboxylic acid diethyl ester (1539-44-2)

Guidance literature:

With ammonium acetate; at 90 ℃; under 760.051 Torr; Time;

DOI:10.1016/j.crci.2012.10.005

Reference yield:

C38H30N8 (61171-83-3) + diethyl 1,4-dihydro-2,4,6-trimethylpyridine-3,5-dicarboxylate (632-93-9) → 2,4-Bis-(N',N'-diphenyl-hydrazino)-6-piperidin-1-yl-benzene-1,3,5-tricarbonitrile (61360-76-7) + 2,4,6-trimethylpyridine-3,5-dicarboxylic acid diethyl ester (1150-55-6)

Guidance literature:

In benzonitrile; at 20 ℃; Rate constant;

upstream raw materials:

C₃₈H₃₀N₈

diethyl 1,4-dihydro-2,4,6-trimethylpyridine-3,5-dicarboxylate

1,3,5-(2,4,6-Tricyanobenzotriyl)tris(N¹,N¹-diphenylhydrazyl)-Triradikal

N_.N-Diphenyl-N'-(3.5-dichlor-2.4.6-tricyan-phenyl)-hydrazyl

Downstream raw materials:

3,5-bis-hydroxymethyl-2,4,6-trimethyl-pyridine

2,4,5-trimethyl-3-ethoxycarbonylpyrrole

diethyl 1,4-dihydro-2,4,6-trimethylpyridine-3,5-dicarboxylate

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