2-Buten-1-one, 1-(2,6,6-trimethyl-2-cyclohexen-1-yl)-, (2E)-

Base Information

Chemical Name:2-Buten-1-one, 1-(2,6,6-trimethyl-2-cyclohexen-1-yl)-, (2E)-
CAS No.:43052-87-5
Molecular Formula:C₁₃H₂₀O
Molecular Weight:192.301
Hs Code.:2914299000
European Community (EC) Number:245-845-8,620-558-4
DSSTox Substance ID:DTXSID0052097
Mol file:43052-87-5.mol

Synonyms:2-Buten-1-one, 1-(2,6,6-trimethyl-2-cyclohexen-1-yl)-;23726-94-5;DTXSID0052097;FT-0622140;FT-0692293;2,6,6-trimethyl-1-(but-2-enoyl)-cyclohex-2-ene;1-(2,6,6-trimethylcyclohex-2-en-1-yl) but-2-en-1-one

Suppliers and Price of 2-Buten-1-one, 1-(2,6,6-trimethyl-2-cyclohexen-1-yl)-, (2E)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
1-(2,6,6-Trimethylcyclohex-2-en-1-yl)but-2-en-1-one 90%
500mg
$ 113.00

Matrix Scientific
1-(2,6,6-Trimethylcyclohex-2-en-1-yl)but-2-en-1-one 90%
250mg
$ 74.00

Matrix Scientific
1-(2,6,6-Trimethylcyclohex-2-en-1-yl)but-2-en-1-one 90%
1g
$ 174.00

Crysdot
1-(2,6,6-Trimethylcyclohex-2-en-1-yl)but-2-en-1-one 95+%
1g
$ 160.00

Crysdot
1-(2,6,6-Trimethylcyclohex-2-en-1-yl)but-2-en-1-one 95+%
5g
$ 450.00

Chemenu
1-(2,6,6-Trimethylcyclohex-2-en-1-yl)but-2-en-1-one 95%
5g
$ 421.00

AK Scientific
alpha-Damascone
1g
$ 49.00

AHH
4-(2.6.6-Trimethylcyclohex-2-enyl)-but-2-en-4-one 97%
5g
$ 768.00

Total 51 raw suppliers

Chemical Property of 2-Buten-1-one, 1-(2,6,6-trimethyl-2-cyclohexen-1-yl)-, (2E)-

Chemical Property:

Vapor Pressure:0.0083mmHg at 25°C
Refractive Index:1.471
Boiling Point:267.1 °C at 760 mmHg
Flash Point:105.7 °C
PSA：17.07000
Density:0.898 g/cm³
LogP:3.51410
XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:192.151415257
Heavy Atom Count:14
Complexity:282

Purity/Quality:

99% ^*data from raw suppliers

1-(2,6,6-Trimethylcyclohex-2-en-1-yl)but-2-en-1-one 90% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC=CC(=O)C1C(=CCCC1(C)C)C

Technology Process of 2-Buten-1-one, 1-(2,6,6-trimethyl-2-cyclohexen-1-yl)-, (2E)-

There total 20 articles about 2-Buten-1-one, 1-(2,6,6-trimethyl-2-cyclohexen-1-yl)-, (2E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.7%

: 39900-15-7
(+/-)-3-hydroxy-1-(2,6,6-trimethylcyclohex-2-en-1-yl)butan-1-one

: 57549-92-5,57549-93-6,43052-87-5
⁽²⁾-1-(2,6,6-trimethylcyclohex-2-en-1-yl)butan-1-one

Guidance literature:: With acetic acid; In toluene; at 60 ℃; for 4h;

Reference yield: 83.0%

: 28102-24-1,28102-25-2,52610-46-5,145774-37-4,148021-15-2,148021-16-3
(Z)-2,6,6-Trimethyl-α-(1-propenyl)-2-cyclohexene-1-methanol

: 127-41-3,6901-97-9,14398-36-8,24190-29-2,30685-95-1,31798-12-6,52340-45-1,67529-94-6,67529-95-7
alpha-ionone

: 57549-92-5,57549-93-6,43052-87-5
⁽²⁾-1-(2,6,6-trimethylcyclohex-2-en-1-yl)butan-1-one

Guidance literature:: With Dess-Martin periodane; In dichloromethane; Ambient temperature;
DOI:10.1016/S0040-4020(01)81022-X

Reference yield: 71.0%

: 61899-98-7
2,6,6-trimethylcyclohex-2-en-1-ylidene ketene

: 107-05-1
3-chloroprop-1-ene

: 57549-92-5,57549-93-6,43052-87-5
⁽²⁾-1-(2,6,6-trimethylcyclohex-2-en-1-yl)butan-1-one

Guidance literature:: 3-chloroprop-1-ene; With magnesium; In tetrahydrofuran; at 20 - 42 ℃; for 1h;

2,6,6-trimethylcyclohex-2-en-1-ylidene ketene; In tetrahydrofuran; at 25 ℃; for 1h;

With toluene-4-sulfonic acid; In ethyl acetate; for 12h; Inert atmosphere; Reflux;