pentacarbonyl{μ-{(η2:η2-ethynyl)benzene}}(trimethyl phosphite)dicobalt-(Co-Co)

Base Information

Chemical Name:pentacarbonyl{μ-{(η2:η2-ethynyl)benzene}}(trimethyl phosphite)dicobalt-(Co-Co)
CAS No.:84896-09-3
Molecular Formula:C₁₆H₁₅Co₂O₈P
Molecular Weight:484.25
Hs Code.:

Synonyms:pentacarbonyl{μ-{(η2:η2-ethynyl)benzene}}(trimethyl phosphite)dicobalt-(Co-Co)

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Chemical Property of pentacarbonyl{μ-{(η2:η2-ethynyl)benzene}}(trimethyl phosphite)dicobalt-(Co-Co)

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Technology Process of pentacarbonyl{μ-{(η2:η2-ethynyl)benzene}}(trimethyl phosphite)dicobalt-(Co-Co)

There total 2 articles about pentacarbonyl{μ-{(η2:η2-ethynyl)benzene}}(trimethyl phosphite)dicobalt-(Co-Co) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 12154-91-5
(phenylacetylene)hexacarbonyldicobalt

: 121-45-9
phosphorous acid trimethyl ester

: 84896-09-3
pentacarbonyl{μ-{(η2:η2-ethynyl)benzene}}(trimethyl phosphite)dicobalt-(Co-Co)

Guidance literature:: In hexane; inert gas; 3 h; boiling hexane; solvent was removed; chromatographed;
DOI:10.1021/ja00345a037

Reference yield: 49.0%

: 12154-91-5
(phenylacetylene)hexacarbonyldicobalt

: 121-45-9
phosphorous acid trimethyl ester

: 123745-44-8
tetracarbonyl{μ-{(η2:η2-ethynyl)benzene}}-bis(trimethyl phosphite)-dicobalt(Co-Co)

: 84896-09-3
pentacarbonyl{μ-{(η2:η2-ethynyl)benzene}}(trimethyl phosphite)dicobalt-(Co-Co)

Guidance literature:: In hexane; (N2); reflux the mixt. for 2-4 h;; concg. the soln. after filtration; chromy. (alumina column, diethyl ether/light petroleum); elem. anal.;
DOI:10.1016/0022-328X(88)87050-5

Reference yield: 6.0%

: 1708-29-8
2,5-dihydrofuran

: 84896-09-3
pentacarbonyl{μ-{(η2:η2-ethynyl)benzene}}(trimethyl phosphite)dicobalt-(Co-Co)

: 122422-20-2
1,3,3a,6a-tetrahydro-5-phenyl-4H-cyclopentafuran-4-one

Guidance literature:: In toluene; (N2); reflux the mixt. for 16 h;; filtration; evapn. of soln.; chromy. of residue (alumina column, CHCl3); solvent removal; elem. anal.;
DOI:10.1016/0022-328X(88)87050-5