gallium(III) meso-tetraphenylporphyrine chloride

Base Information

Chemical Name:gallium(III) meso-tetraphenylporphyrine chloride
CAS No.:78833-52-0
Molecular Formula:C₄₄H₂₈ClGaN₄
Molecular Weight:717.909
Hs Code.:

Synonyms:gallium(III) meso-tetraphenylporphyrine chloride

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Chemical Property of gallium(III) meso-tetraphenylporphyrine chloride

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Technology Process of gallium(III) meso-tetraphenylporphyrine chloride

There total 7 articles about gallium(III) meso-tetraphenylporphyrine chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 105796-33-6
(OAc)GaTPP

: 78833-52-0
gallium(III) meso-tetraphenylporphyrine chloride

Guidance literature:: In hydrogenchloride; Ga compd. in 33% HCl boiled for 3 h; solvent removed in vac.; dissolved in small amt. of CHCl3; washed with water; dried (CaCl2); repeatedly chromd. (Al2O3, CHCl3); solvent distd. off in vac.;
DOI:10.1023/A:1023455325461

Reference yield: 85.0%

: 917-23-7,20998-75-8
5,10,15,20-tetraphenyl-21H,23H-porphine

: 13450-90-3
Gallium trichloride

: 78833-52-0
gallium(III) meso-tetraphenylporphyrine chloride

Guidance literature:: With sodium acetate; In acetic acid; porphyrin soln. in AcOH adding dropwise under inert atm. to GaCl3 soln.in AcOH, then AcONa in AcOH adding, refluxing for 24 h, cooling to roomtemp., solid collecting and drying; purified by recrystallization from toluene-heptane; identified by elem.anal., UV and NMR spectra;
DOI:10.1016/S0022-328X(00)99222-2

Reference yield: 71.0%

: 917-23-7,20998-75-8
5,10,15,20-tetraphenyl-21H,23H-porphine

: 13450-90-3
Gallium trichloride

: 78833-52-0
gallium(III) meso-tetraphenylporphyrine chloride

: acetato-(5,10,15,20-tetraphenylporphyrinato)gallium(III)

Guidance literature:: With sodium acetate; In acetic acid; addn. of sodium acetate soln. to soln. of porphyrin and GaCl3, refluxing, 12h; cooling to 0°C; pptn.; recrystn. (toluene); elem. anal.;
DOI:10.1016/S0277-5387(00)81386-8