1,1,1,3,3,3-Hexamethyl-2-(4-phenyl-4-trimethylsilanyloxy-but-2-ynyl)-disilazane

Base Information

Chemical Name:1,1,1,3,3,3-Hexamethyl-2-(4-phenyl-4-trimethylsilanyloxy-but-2-ynyl)-disilazane
CAS No.:91375-45-0
Molecular Formula:C₁₉H₃₅NOSi₃
Molecular Weight:377.75
Hs Code.:

Synonyms:1,1,1,3,3,3-Hexamethyl-2-(4-phenyl-4-trimethylsilanyloxy-but-2-ynyl)-disilazane

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Chemical Property of 1,1,1,3,3,3-Hexamethyl-2-(4-phenyl-4-trimethylsilanyloxy-but-2-ynyl)-disilazane

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Technology Process of 1,1,1,3,3,3-Hexamethyl-2-(4-phenyl-4-trimethylsilanyloxy-but-2-ynyl)-disilazane

There total 5 articles about 1,1,1,3,3,3-Hexamethyl-2-(4-phenyl-4-trimethylsilanyloxy-but-2-ynyl)-disilazane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 91375-25-6
1,1,1,3,3,3-hexamethyl-2-(prop-2-ynyl)disilazane

: 91375-45-0
1,1,1,3,3,3-Hexamethyl-2-(4-phenyl-4-trimethylsilanyloxy-but-2-ynyl)-disilazane

Guidance literature:: Multi-step reaction with 2 steps

1: MeLi / diethyl ether

2: 1.) -78 to 20 deg C, THF; 2.) 20 deg C, 24 h

With methyllithium; In diethyl ether;
DOI:10.1016/S0040-4039(01)90067-X

Reference yield:

: 999-97-3
1,1,1,3,3,3-hexamethyl-disilazane

: 91375-45-0
1,1,1,3,3,3-Hexamethyl-2-(4-phenyl-4-trimethylsilanyloxy-but-2-ynyl)-disilazane

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi, 2.) H₂O, phosphate buffer / 1.) Et₂O, overnight

With n-butyllithium; phosphate buffer; water;
DOI:10.1016/S0040-4020(01)88215-6

Reference yield:

: 4039-32-1
lithium hexamethyldisilazane

: 91375-45-0
1,1,1,3,3,3-Hexamethyl-2-(4-phenyl-4-trimethylsilanyloxy-but-2-ynyl)-disilazane

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether

2: 1.) -78 to 20 deg C, THF; 2.) 20 deg C, 24 h

In diethyl ether;
DOI:10.1016/S0040-4039(01)90067-X