methyl 2-(tert butoxy)-2-(2-chloro-5-nitro-4-phenoxyphenyl)acetate

Base Information

Chemical Name:methyl 2-(tert butoxy)-2-(2-chloro-5-nitro-4-phenoxyphenyl)acetate
CAS No.:1402890-92-9
Molecular Formula:C₁₉H₂₀ClNO₆
Molecular Weight:393.824
Hs Code.:

Synonyms:methyl 2-(tert butoxy)-2-(2-chloro-5-nitro-4-phenoxyphenyl)acetate

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Chemical Property of methyl 2-(tert butoxy)-2-(2-chloro-5-nitro-4-phenoxyphenyl)acetate

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Technology Process of methyl 2-(tert butoxy)-2-(2-chloro-5-nitro-4-phenoxyphenyl)acetate

There total 7 articles about methyl 2-(tert butoxy)-2-(2-chloro-5-nitro-4-phenoxyphenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1402890-91-8
methyl 2-(tert-butoxy)-2-(2-chloro-4-fluoro-5-nitrophenyl)acetate

: 108-95-2,27073-41-2
phenol

: 1402890-92-9
methyl 2-(tert butoxy)-2-(2-chloro-5-nitro-4-phenoxyphenyl)acetate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 75 ℃; for 4h;

Reference yield:

: 110322-88-8
2'-chloro-4'-fluoro-5'-nitroacetophenone

: 1402890-92-9
methyl 2-(tert butoxy)-2-(2-chloro-5-nitro-4-phenoxyphenyl)acetate

Guidance literature:: Multi-step reaction with 4 steps

1: selenium(IV) oxide; ytterbium(III) triflate / 1,4-dioxane; water / 48 h / 90 °C

2: sulfuric acid / 3 h / Reflux

3: perchloric acid / 3 h / -20 - 20 °C

4: potassium carbonate / N,N-dimethyl-formamide / 4 h / 75 °C

With selenium(IV) oxide; perchloric acid; sulfuric acid; potassium carbonate; ytterbium(III) triflate; In 1,4-dioxane; water; N,N-dimethyl-formamide;

Reference yield:

: 2252-51-9
2-choro-4-fluorobenzoic acid

: 1402890-92-9
methyl 2-(tert butoxy)-2-(2-chloro-5-nitro-4-phenoxyphenyl)acetate

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium nitrate; sulfuric acid / 6 h / 0 - 20 °C

2.1: thionyl chloride / 2 h / Reflux

3.1: triethylamine; ethyl potassium malonate; magnesium chloride / acetonitrile / 20 °C

3.2: Reflux

4.1: selenium(IV) oxide; ytterbium(III) triflate / 1,4-dioxane; water / 48 h / 90 °C

5.1: sulfuric acid / 3 h / Reflux

6.1: perchloric acid / 3 h / -20 - 20 °C

7.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 75 °C

With selenium(IV) oxide; thionyl chloride; perchloric acid; sulfuric acid; ethyl potassium malonate; potassium carbonate; potassium nitrate; triethylamine; magnesium chloride; ytterbium(III) triflate; In 1,4-dioxane; water; N,N-dimethyl-formamide; acetonitrile;