6-(3-(2-[2-(2-phenyl-1-ethynyl)-1-cyclohexenyl]-1-ethynyl)-phenyl)-5-hexynoic acid

Base Information

Chemical Name:6-(3-(2-[2-(2-phenyl-1-ethynyl)-1-cyclohexenyl]-1-ethynyl)-phenyl)-5-hexynoic acid
CAS No.:303142-43-0
Molecular Formula:C₂₈H₂₄O₂
Molecular Weight:392.497
Hs Code.:

Synonyms:6-(3-(2-[2-(2-phenyl-1-ethynyl)-1-cyclohexenyl]-1-ethynyl)-phenyl)-5-hexynoic acid

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Chemical Property of 6-(3-(2-[2-(2-phenyl-1-ethynyl)-1-cyclohexenyl]-1-ethynyl)-phenyl)-5-hexynoic acid

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Technology Process of 6-(3-(2-[2-(2-phenyl-1-ethynyl)-1-cyclohexenyl]-1-ethynyl)-phenyl)-5-hexynoic acid

There total 10 articles about 6-(3-(2-[2-(2-phenyl-1-ethynyl)-1-cyclohexenyl]-1-ethynyl)-phenyl)-5-hexynoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 871927-80-9
methyl 6-(3-(2-[2-(2-phenyl-1-ethynyl)-1-cyclohexenyl]-1-ethynyl)-phenyl)-5-hexynoate

: 303142-43-0
6-(3-(2-[2-(2-phenyl-1-ethynyl)-1-cyclohexenyl]-1-ethynyl)-phenyl)-5-hexynoic acid

Guidance literature:: With lithium hydroxide; In water; at 0 - 20 ℃; for 6h;
DOI:10.1021/jo051403q

Reference yield:

: 77758-51-1
methyl hex-5-ynoate

: 303142-43-0
6-(3-(2-[2-(2-phenyl-1-ethynyl)-1-cyclohexenyl]-1-ethynyl)-phenyl)-5-hexynoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / n-butylamine; CuI / PdCl₂(PPh₃)2 / diethyl ether / 4 h / 0 - 20 °C

2: 94 percent / triethylamine; CuI / Pd(PPh₃)2 / 4 h

3: 89 percent / LiOH*H₂O / H₂O / 6 h / 0 - 20 °C

With lithium hydroxide; copper(l) iodide; N-butylamine; triethylamine; bis-triphenylphosphine-palladium(II) chloride; bis(triphenylphosphine)palladium⁽⁰⁾; In diethyl ether; water;
DOI:10.1021/jo051403q

Reference yield:

: 303142-41-8
methyl 6-(3-iodophenyl)-5-hexynoate

: 303142-43-0
6-(3-(2-[2-(2-phenyl-1-ethynyl)-1-cyclohexenyl]-1-ethynyl)-phenyl)-5-hexynoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / triethylamine; CuI / Pd(PPh₃)2 / 4 h

2: 89 percent / LiOH*H₂O / H₂O / 6 h / 0 - 20 °C

With lithium hydroxide; copper(l) iodide; triethylamine; bis(triphenylphosphine)palladium⁽⁰⁾; In water;
DOI:10.1021/jo051403q