(2S)-2-amino-3-(4-methoxyphenyl)-2-methylpropionamide formic acid salt

Base Information

Chemical Name:(2S)-2-amino-3-(4-methoxyphenyl)-2-methylpropionamide formic acid salt
CAS No.:1299492-20-8
Molecular Formula:CH₂O₂*C₁₁H₁₆N₂O₂
Molecular Weight:254.286
Hs Code.:

Synonyms:(2S)-2-amino-3-(4-methoxyphenyl)-2-methylpropionamide formic acid salt

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Chemical Property of (2S)-2-amino-3-(4-methoxyphenyl)-2-methylpropionamide formic acid salt

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Technology Process of (2S)-2-amino-3-(4-methoxyphenyl)-2-methylpropionamide formic acid salt

There total 3 articles about (2S)-2-amino-3-(4-methoxyphenyl)-2-methylpropionamide formic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 64-18-6
formic acid

: 1299492-08-2
2-[(R)-(carbamoylphenylmethyl)-amino]-3-(4-methoxyphenyl)-2-(S)-methylpropionamide

: 1299492-20-8
(2S)-2-amino-3-(4-methoxyphenyl)-2-methylpropionamide formic acid salt

: 103-81-1
Benzeneacetamide

Guidance literature:: palladium on carbon; In methanol; water; at 20 - 60 ℃; for 5.75h;

Reference yield:

: 122-84-9
4-methoxybenzyl methyl ketone

: 1299492-20-8
(2S)-2-amino-3-(4-methoxyphenyl)-2-methylpropionamide formic acid salt

Guidance literature:: Multi-step reaction with 3 steps

1.1: water; methanol / 20 h / 40 °C / Sealed tube

2.1: sulfuric acid / dichloromethane; water / 3.25 h / -10 - 0 °C / Cooling with ice

2.2: pH 8 - 9

3.1: palladium on carbon / water; methanol / 5.75 h / 20 - 60 °C

With sulfuric acid; palladium on carbon; In methanol; dichloromethane; water;

Reference yield:

: 1299492-07-1
2-[1-(S)-cyano-2-(4-methoxyphenyl)-1-methylethylamino]-2-(R)-phenylacetamide

: 1299492-20-8
(2S)-2-amino-3-(4-methoxyphenyl)-2-methylpropionamide formic acid salt

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfuric acid / dichloromethane; water / 3.25 h / -10 - 0 °C / Cooling with ice

1.2: pH 8 - 9

2.1: palladium on carbon / water; methanol / 5.75 h / 20 - 60 °C

With sulfuric acid; palladium on carbon; In methanol; dichloromethane; water;