phenylmethyl 4-[4-(4-piperidinyloxy)phenyl]-1-piperidinecarboxylate

Base Information Edit

Chemical Name:phenylmethyl 4-[4-(4-piperidinyloxy)phenyl]-1-piperidinecarboxylate
CAS No.:915199-12-1
Molecular Formula:C₂₄H₃₀N₂O₃
Molecular Weight:394.514
Hs Code.:
Mol file:915199-12-1.mol

Synonyms:phenylmethyl 4-[4-(4-piperidinyloxy)phenyl]-1-piperidinecarboxylate

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Chemical Property of phenylmethyl 4-[4-(4-piperidinyloxy)phenyl]-1-piperidinecarboxylate Edit

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Technology Process of phenylmethyl 4-[4-(4-piperidinyloxy)phenyl]-1-piperidinecarboxylate

There total 2 articles about phenylmethyl 4-[4-(4-piperidinyloxy)phenyl]-1-piperidinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 778642-37-8
phenylmethyl 4-{4-[(1-{[(1,1-dimethylethyl)oxy]carbonyl}-4-piperidinyl)oxy]phenyl}-4-hydroxy-1-piperidinecarboxylate

: 915199-12-1
phenylmethyl 4-[4-(4-piperidinyloxy)phenyl]-1-piperidinecarboxylate

Guidance literature:: With triethylsilane; trifluoroacetic acid; In dichloromethane; at -78 - 20 ℃;

Reference yield:

: 109384-19-2
t-butyl 4-hydroxy piperidine-1-carboxylate

: 915199-12-1
phenylmethyl 4-[4-(4-piperidinyloxy)phenyl]-1-piperidinecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: di-tert-butyl-diazodicarboxylate; triphenylphosphine / dichloromethane / 65 h / 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -75 - -70 °C

2.2: -70 - 20 °C

3.1: triethylsilane; trifluoroacetic acid / dichloromethane / -78 - 20 °C

With triethylsilane; n-butyllithium; di-tert-butyl-diazodicarboxylate; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; hexane; dichloromethane;