(S)-3-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecoxy)phenyl]-2-(methanesulfonylamino)propyl methanesulfonate

Base Information

Chemical Name:(S)-3-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecoxy)phenyl]-2-(methanesulfonylamino)propyl methanesulfonate
CAS No.:1068142-17-5
Molecular Formula:C₂₂H₂₂F₁₇NO₆S₂
Molecular Weight:783.525
Hs Code.:

Synonyms:(S)-3-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecoxy)phenyl]-2-(methanesulfonylamino)propyl methanesulfonate

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Chemical Property of (S)-3-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecoxy)phenyl]-2-(methanesulfonylamino)propyl methanesulfonate

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Technology Process of (S)-3-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecoxy)phenyl]-2-(methanesulfonylamino)propyl methanesulfonate

There total 5 articles about (S)-3-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecoxy)phenyl]-2-(methanesulfonylamino)propyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1068142-16-4
(S)-2-(tert-butoxycarbonylamino)-3-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecoxy) phenyl]-1-propanol

: 124-63-0
methanesulfonyl chloride

: 1068142-17-5
(S)-3-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecoxy)phenyl]-2-(methanesulfonylamino)propyl methanesulfonate

Guidance literature:: (S)-2-(tert-butoxycarbonylamino)-3-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecoxy) phenyl]-1-propanol; With hydrogenchloride; In ethyl acetate;

methanesulfonyl chloride; With triethylamine; In tetrahydrofuran; at 20 ℃; for 17h; Further stages.;
DOI:10.1016/j.tetlet.2008.07.125

Reference yield:

: C₂₀H₁₈F₁₇NO₂

: 124-63-0
methanesulfonyl chloride

: 1068142-17-5
(S)-3-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecoxy)phenyl]-2-(methanesulfonylamino)propyl methanesulfonate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.tet.2015.09.024

Reference yield:

: 83345-46-4,282100-80-5
N-(tert-butyloxycarbonyl)-L-tyrosinol

: 1068142-17-5
(S)-3-[4-(4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecoxy)phenyl]-2-(methanesulfonylamino)propyl methanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetonitrile / 24 h / 70 °C

2: hydrogenchloride; water / ethyl acetate / 3 h / 20 °C

3: triethylamine / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

With hydrogenchloride; water; potassium carbonate; triethylamine; In tetrahydrofuran; ethyl acetate; acetonitrile;
DOI:10.1016/j.tet.2015.09.024