2,4,6-Tris(2,4,6-tribromophenoxy)-1,3,5-triazine

Base Information

• Chemical Name: 2,4,6-Tris(2,4,6-tribromophenoxy)-1,3,5-triazine
• CAS No.: 25713-60-4
• Deprecated CAS: 157971-54-5,136991-02-1
• Molecular Formula: C21 H6 Br9 N3 O3
• Molecular Weight: 1067.43
• Hs Code.: 29336990
• European Community (EC) Number: 426-040-2,607-784-9
• UNII: QKS4PD9ZS8
• DSSTox Substance ID: DTXSID0058695
• Nikkaji Number: J948.093E
• Wikidata: Q19931409
• Mol file: 25713-60-4.mol

Synonyms:2,4,6-tris(2,4,6-tribromophenoxy)-1,3,5-triazine;TTBP-TAZ

Chemical Property of 2,4,6-Tris(2,4,6-tribromophenoxy)-1,3,5-triazine

Chemical Property:

• Appearance/Colour: white powder
• Vapor Pressure: 2.02E-25mmHg at 25°C
• Melting Point: 230 °C
• Refractive Index: 1.723
• Boiling Point: 812.2 °C at 760 mmHg
• PKA: -2.43±0.10(Predicted)
• Flash Point: 445 °C
• PSA: 66.36000
• Density: 2.502 g/cm³
• LogP: 12.11100
• Storage Temp.: Sealed in dry,Room Temperature
• Solubility.: Chloroform (Slightly), Dichloromethane (Slightly)
• Water Solubility.: 1μg/L at 20℃
• XLogP3: 11.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 6
• Exact Mass: 1066.29776
• Heavy Atom Count: 36
• Complexity: 582

Purity/Quality:

bromine,67%min. ^*data from raw suppliers

2,4,6-Tris(2,4,6-tribomophenoxy)-1,3,5-triazine ^*data from reagent suppliers

Safty Information:

• Safety Statements: 24/25

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=C(C=C(C(=C1Br)OC2=NC(=NC(=N2)OC3=C(C=C(C=C3Br)Br)Br)OC4=C(C=C(C=C4Br)Br)Br)Br)Br
• Uses: Tris(tribromophenyl) Cyanurate acts as a novel brominated flame retardant.

Technology Process of 2,4,6-Tris(2,4,6-tribromophenoxy)-1,3,5-triazine

There total 4 articles about 2,4,6-Tris(2,4,6-tribromophenoxy)-1,3,5-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

1,3,5-trichloro-2,4,6-triazine (108-77-0) + 2,4,6-tribromophenol (118-79-6) + phenol (108-95-2,27073-41-2) → 2,4,6-tris(2,4,6-tribromophenoxy)-1,3,5-triazine (25713-60-4)

Guidance literature:

With sodium hydroxide; hydrogen bromide; bromine; hydrazine; In water; acetone;

Reference yield: 98.0%

1-methyl-1H-imidazole (616-47-7) + 1,3,5-trichloro-2,4,6-triazine (108-77-0) + 2,4,6-tribromophenol (118-79-6) → 2,4,6-tris(2,4,6-tribromophenoxy)-1,3,5-triazine (25713-60-4)

Guidance literature:

1-methyl-1H-imidazole; 2,4,6-tribromophenol; In chlorobenzene; at 40 ℃; for 2h;

1,3,5-trichloro-2,4,6-triazine; In chlorobenzene; at 20 - 25 ℃; for 4h; Temperature;

Reference yield: 98.0%

1,3,5-trichloro-2,4,6-triazine (108-77-0) + 2,4,6-tribromophenol (118-79-6) → 2,4,6-tris(2,4,6-tribromophenoxy)-1,3,5-triazine (25713-60-4)

Guidance literature:

With magnesium silicate; sodium hydroxide; sodium sulfite; trimethylamine; In dichloromethane; water; at 3 - 30 ℃; Product distribution / selectivity; Reflux;

upstream raw materials:

1,3,5-trichloro-2,4,6-triazine

2,4,6-tribromophenol

phenol

1-methyl-1H-imidazole

Refernces

• 1、 -. "FLAME RETARDANT COMPOSITION FORFLAMMABLE PLASTIC MATERIALS COMPRISING2,4,6-TRIS(2,4,6-TRIBROMOPHENOXY)-1,3,5-TRIAZINE AND PROCESSFOR PRODUCING THE SAME". Page/Page column 9. . Retrieved 2010/11/17.
• 2、 -. "Production of tris(2,4,6-tribromophenoxy)-s-1,3,5-triazine". . . Retrieved 2008/06/13.