1-adamantyl 4-amino>phenyl carbonate

Base Information

Chemical Name:1-adamantyl 4-amino>phenyl carbonate
CAS No.:172973-98-7
Molecular Formula:C₂₃H₃₃NO₉S₂
Molecular Weight:531.648
Hs Code.:

1-adamantyl 4-<bis<2-(mesyloxy)ethyl>amino>phenyl carbonate

Synonyms:1-adamantyl 4-amino>phenyl carbonate

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Chemical Property of 1-adamantyl 4-amino>phenyl carbonate

Chemical Property:

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Technology Process of 1-adamantyl 4-amino>phenyl carbonate

There total 3 articles about 1-adamantyl 4-amino>phenyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 124-63-0
methanesulfonyl chloride

: 172973-90-9
Carbonic acid adamantan-1-yl ester 4-[bis-(2-hydroxy-ethyl)-amino]-phenyl ester

: 1-adamantyl 4-phenyl carbonate

: 172973-94-3
1-adamantyl 4-<(2-chloroethyl)<2-(mesyloxy)ethyl>amino>phenyl carbonate

: 172973-98-7
1-adamantyl 4-amino>phenyl carbonate

Guidance literature:: With pyridine; a) 0 deg C, 40 min, b) 50 deg C, 18 min;
DOI:10.1021/jm00026a013

Reference yield:

: 5854-73-9
1-Adamantyl-p-nitrophenyl-carbonat

: 172973-98-7
1-adamantyl 4-amino>phenyl carbonate

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium formate / 10percent Pd/C / ethanol

2: 82 percent / AcOH / 48 h / Ambient temperature

3: 48 percent / pyridine / a) 0 deg C, 40 min, b) 50 deg C, 18 min

With pyridine; ammonium formate; acetic acid; palladium on activated charcoal; In ethanol;
DOI:10.1021/jm00026a013

Reference yield:

: 172974-25-3
Carbonic acid adamantan-1-yl ester 4-amino-phenyl ester

: 172973-98-7
1-adamantyl 4-amino>phenyl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / AcOH / 48 h / Ambient temperature

2: 48 percent / pyridine / a) 0 deg C, 40 min, b) 50 deg C, 18 min

With pyridine; acetic acid;
DOI:10.1021/jm00026a013